High-temperature-resistant adhesive-blocking release film for flexible circuit board, and preparation method and application thereof
A flexible circuit board, high temperature resistant technology, applied in the direction of chemical instruments and methods, coatings, layered products, etc., can solve the problems of increased process steps, high price, low water absorption, etc., and achieve simple preparation methods and low raw material costs , the effect of mild conditions
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[0065] The present invention also provides a method for preparing the high temperature resistant adhesive release film described in the above technical solution, comprising the following steps:
[0066] a) Fully disperse, mix and filter the fluorocarbon resin, fluorine release agent and organic solvent to obtain the main agent; then compound the main agent and curing agent to obtain a fluorine release coating; the fluorine release The agent is selected from at least one of fluorine-containing polyacrylate and PTFE;
[0067] b) coating the fluorine release coating obtained in step a) on the substrate, curing, cooling and winding to obtain a high temperature resistant adhesive release film.
[0068] In the invention, firstly, the fluorocarbon resin, the fluorine release agent and the organic solvent are fully dispersed, mixed and filtered to obtain the main agent. In the present invention, the fluorocarbon resin, fluorine release agent and organic solvent are the same as those ...
Embodiment 1
[0081] (1) In 1180 parts by weight of ethyl acetate solvent, add 300 parts by weight of tetrafluoroethylene-vinyl ether copolymer (Huarin: HLR-6, solid content 65%), 39 parts by weight of fluorine-containing polyacrylic acid Esters (AG: PM4800, 3M), fully dispersed, mixed and filtered to obtain the main agent of fluorine release coating.
[0082] (2) Select TPA-100 (Asahi Glass, 100% solid content) as the curing agent, add 130 parts by weight to the main agent of the fluorine release coating obtained in step (1) for compounding, and disperse at 900rpm for 20min to obtain fluorine Plain release coating.
[0083] (3) Adopt anilox coating production line, coat the fluorine release coating obtained in step (2) on the PET film (width is 1040 mm, thickness is 50 μm), set the coating thickness, wet film thickness is 30 μm, coat The line speed of the cloth production line is 10m / min; the oven length of the anilox coating production line is 30m, and there are 10 sections in total. ...
Embodiment 2
[0085](1) Add 150 parts by weight of PTFE micropowder in 500 parts by weight of methyl ethyl ketone solvent, and soak for 1h to 2h; then add 300 parts by weight of tetrafluoroethylene-vinyl ether copolymer (Hualin : HLR-6, solid content 65%), after fully dispersing, mixing and filtering, the main agent of fluorine release coating is obtained.
[0086] (2) Select TPA-100 (Asahi Glass, 100% solid content) as the curing agent, add 130 parts by weight to the main agent of the fluorine release coating obtained in step (1) for compounding, and disperse at 900rpm for 20min to obtain fluorine Plain release coating.
[0087] (3) Adopt anilox coating production line, coat the fluorine release coating obtained in step (2) on the PET film (width is 1040mm, thickness is 75μm), set the coating thickness, wet film thickness is 30μm, coat The line speed of the cloth production line is 10m / min; the oven length of the anilox coating production line is 30m, and there are 10 sections in total....
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