Radiation-resistant additive and synthesis thereof, and method for preparing radiation-resistant silicone rubber material
A technology of radiation resistance and additives, which is applied in the field of preparation of radiation-resistant silicone rubber materials to achieve the effect of improving radiation resistance and good compatibility
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[0028] Below in conjunction with embodiment technical scheme of the present invention is described in further detail:
[0029] The steps of the preparation method of the silazane damping agent containing triphenylsiloxane structure are:
[0030] (1) Preparation for synthesis
[0031] Molecular sieves are dried in a box-type resistance furnace at 400°C for 3.0 hours, put into a desiccator to cool, then put dry molecular sieves into a container containing toluene, and place them for more than 2 days before use; the glass instruments and stirring After the rod is cleaned, put it into the oven, set the temperature of the oven at 120°C, bake for 2 hours, and wait for use after cooling. The glass instrument includes a four-necked reaction bottle, an air guide tube, a reflux condenser, and a constant pressure dripping device.
[0032] (2) intermediate synthesis reaction
[0033] Install a stirring device at the middle port of the four-necked reaction bottle, install an air guide pi...
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