Extreme-pressure-resistant anti-wear agent and preparation method thereof
An extreme pressure antiwear agent, polar technology, applied in the direction of additives, petroleum industry, lubricating composition, etc., can solve the problem that antiwear agent can not reduce friction loss, etc., to reduce steric effect, increase contact area, and reduce molecular weight Effect
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[0031] The preparation method of viscosity reducing active agent is:
[0032] S1. Take zirconium n-butoxide at a mass ratio of 1~3:2~5 and add cage-type octapoly(trimethylsiloxy)silsesquioxane to mix to obtain a mixture. Take the mixture at a mass ratio of 2~5:10 Add absolute ethanol at ~15 minutes, stir and mix for 20-30 minutes to obtain a mixed solution, take the mixed solution and add it dropwise to deionized water at a mass ratio of 1~3:3~5, control the dropping time for 30~60 minutes, and stir and mix for 2~4 hours , centrifuged, the precipitate was taken and dried, ground and pulverized through an 80-mesh sieve, and the sieved particles were collected;
[0033] S2. Take the sieved particles and add tetraethyl silicate according to the mass ratio of 1~5:10~15, add a catalytic active agent with a quality of 90~95% of tetraethyl silicate, stir and mix for 20~30min to obtain mixture a, take Add deionized water to mixture a according to the mass ratio of 10~15:5~9, stir and...
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