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Curing agent sustained release capsule for gas injection channeling prevention, channeling prevention agent and preparation method of curing agent sustained release capsule

A slow-release capsule and curing agent technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of contradictory wellbore injectability and plugging performance, large fracture and hole size, short validity period, etc., and achieve excellent Wellbore injectability, extended curing time, and good wellbore injectability

Active Publication Date: 2019-06-14
CHINA PETROLEUM & CHEM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Due to the characteristics of high-temperature and high-salt oil reservoirs with a temperature greater than 120°C, formation water salinity greater than 100,000 mg / L, and large fractures and caves, which are centimeter-level, commonly used anti-channeling agents have poor adaptability to high-temperature and high-salt oil reservoirs. The specific performance is: cement has a strong plugging ability, but it is easy to differentiate by gravity and cannot enter the channel of gas channeling. It is easy to degrade under high salt and has a short validity period; the foaming ability of foam anti-channeling agent is greatly affected by shearing, which is more suitable for anti-channeling in sandstone reservoirs, but poor in foaming and plugging ability for fracture-cavity reservoirs
Resin and its composite materials have low density, can flow with gas injection, and have good wellbore injectability, but because of the low density, even if they can successfully reach the target position, they cannot effectively play a plugging role, and there is a wellbore injectability of resin. It is contradictory with the sealing property and cannot be effectively blocked

Method used

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  • Curing agent sustained release capsule for gas injection channeling prevention, channeling prevention agent and preparation method of curing agent sustained release capsule
  • Curing agent sustained release capsule for gas injection channeling prevention, channeling prevention agent and preparation method of curing agent sustained release capsule
  • Curing agent sustained release capsule for gas injection channeling prevention, channeling prevention agent and preparation method of curing agent sustained release capsule

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1-7

[0030] The coating agent, curing agent and hollow glass microspheres are configured according to the proportions of Examples 1-7 in Table 1. Among them, the dry powder of the curing agent for anti-air channeling is selected from urotropine, and the particle size is 200-400 mesh; the coating agent is selected from linear Low-density polyethylene LLDPE particles, the particle size is 1-2mm; the density regulator is hollow glass microspheres, the particle size is 200-400 mesh, and the density is 0.59g / cm 3 , Compressive strength 30 ~ 70MPa.

Embodiment 1

[0031] Taking Example 1 as an example, prepare low-density curing agent sustained-release capsules according to the following methods and steps:

[0032] (1) Take by weighing 20g quality anti-channeling curing agent powder, 22.5g coating agent and 2.5g density regulator;

[0033] (2) Add the coating agent to the 120°C reaction kettle, and heat to completely melt the coating agent;

[0034] (3) Add solidifying agent and density regulator successively to the coating agent of melting and continue to stir, stop heating after making each material mix evenly;

[0035] (4) After the reactor is cooled to room temperature, the materials are taken out, pulverized and granulated to obtain low-density curing agent capsules.

[0036] The prepared low-density curing agent capsules were subjected to a density test, a curing time test and a curing ability test.

[0037] 1. Density test

[0038] Take the coating material (particle size 1-2mm), hollow glass microspheres (particle size 200-40...

Embodiment 8-13

[0046] The coating agent, curing agent and density regulator were configured according to the component ratios of Examples 8-13 in Table 1, and the corresponding curing agent sustained-release capsules were prepared according to the component parameters and preparation conditions of Example 1.

[0047] And the solidifying agent capsule prepared is carried out density test, curing time test and curing ability test according to the test procedure of embodiment 1, and difference is in test condition, thermosetting resin: the mass ratio of curing agent slow-release capsule is 100:8, test The temperature was 115°C. The results are shown in Table 1, wherein the test curve of Example 13 is shown in Figure 3-4 .

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Abstract

The invention discloses a curing agent sustained release capsule for gas injection channeling prevention, a channeling prevention agent and a preparation method of the curing agent sustained release capsule. The curing agent sustained release capsule is prepared from the following components in parts by weight, 20-40 parts of a resin curing agent, 5-35 parts of a density regulator and 45-75 partsof a coating agent, the resin curing agent is sealed in the coating agent, and the density of the curing agent sustained release capsule is 0.66-0.8 g / cm<3>. The preparation method of the curing agentsustained release capsule comprises the following steps that all the components are evenly mixed at the high temperature according to a certain proportion, cooling is conducted to the room temperature, crushing and granulation are conducted, and thus the curing agent sustained release capsule can be obtained. The density of the curing agent sustained release capsule prepared through the preparation method is between the density of water and the density of injected nitrogen, and is closer to the density of the nitrogen, thus the curing agent sustained release capsule can flow along with a gasinjection channel after being mixed with a resin material, the curing agent sustained release capsule has excellent wellbore injectivity and meanwhile has the sustained release action, a curing reaction is generated only when the curing agent sustained release capsule enters the deep part of an oil reservoir, and the excellent plugging property is achieved.

Description

technical field [0001] The invention relates to an anti-gas channeling process in the gas injection flooding technology of high-temperature and high-salt reservoirs, in particular to a curing agent used in a thermosetting resin anti-channeling agent. Background technique [0002] Gas flooding is one of the effective technologies for enhancing oil recovery. During the gas injection process, due to the influence of reservoir heterogeneity, the injected gas often flows along channels with high flow capacity such as fractures, karst caves, or large pores, resulting in low gas injection efficiency, low reservoir recovery, and low oilfield development costs. rise. At present, there is a large demand for gas injection anti-channeling agents in oilfields. On-site injection of anti-channeling agents to chemically block gas channeling channels can effectively alleviate gas injection and gas channeling. Materials used for gas injection anti-channeling in conventional reservoirs inclu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/516C09K8/502
Inventor 胡文革刘中云周福建胡广杰何龙王建海丁保东任波焦保雷冯一波曾文广秦飞魏芳甄恩龙杨利萍
Owner CHINA PETROLEUM & CHEM CORP
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