A kind of emulsified paraffin and its preparation method and application
A technology of emulsified paraffin and paraffin, which is applied in the field of emulsified paraffin and its preparation, which can solve the problems of small improvement, floating phenomenon of emulsified paraffin, delamination, etc., and achieves improved compressive strength, excellent water-reducing effect, and simple dispensing process Effect
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preparation example Construction
[0047] The preparation method of emulsified paraffin is:
[0048] Put the paraffin wax and compound emulsifier prepared according to the designed ratio into the reaction vessel, keep stirring in a water bath at 75°C until the paraffin wax melts, and stir it with an electric mixer at a speed of 800r / min after melting, and divide it at intervals Add deionized water at a temperature of 75°C several times with an interval of 30s until the paraffin phase inversion, then add the remaining deionized water, adjust the stirring speed to 1000r / min, continue stirring for 40min, and then mix the obtained Cool the solution at 4°C to obtain the emulsified paraffin solution;
[0049] In terms of mass ratio, the total amount of water:paraffin=4:1.
Embodiment 1
[0051] The compounding agent in this example includes the following components in parts by weight: Span-80: 90 parts; Tween-80: 40 parts; Pingpingjia A-20: 10 parts; OP-10: 30 parts ; Triethanolamine: 10 parts; Stearic acid: 5 parts; Ethylene glycol, 37 parts. At this time, the HLB value of the composite emulsifier is 9.605, and the mass fraction of the composite emulsifier in the emulsified paraffin wax of this embodiment is 3%.
[0052] The emulsified paraffin wax obtained in Example 1 has good stability, no delamination after centrifugation, and a shelf life of about three months. The dispersion of the emulsion is first-grade, and after drying, a uniform, stable, and strong hydrophobic wax film can be formed. The particle size is Micron level, when mixed into concrete, it has good compatibility with concrete, has a weak effect on cement hydration, and can play a certain role in reducing water, with a water reducing rate of about 6.2%.
[0053] The emulsified paraffin is mi...
Embodiment 2
[0055] The compounding agent in this example includes the following components in parts by weight: Span-80: 92 parts; Tween-80: 42 parts; Pingpingjia A-20: 12 parts; OP-10: 32 parts parts; triethanolamine: 12 parts; stearic acid: 6 parts; ethylene glycol, 40 parts. At this time, the HLB value of the composite emulsifier is 9.769, and the mass fraction of the composite emulsifier in the emulsified paraffin wax of this embodiment is 3%.
[0056] The emulsified paraffin wax obtained in Example 2 has good stability, no delamination after centrifugation, and a shelf life of about three months. The dispersion of the emulsion is first-grade, and after drying, a uniform, stable, and strong hydrophobic wax film can be formed. The particle size is Micron level, when mixed into concrete, it has good compatibility with concrete, has a weak effect on cement hydration, and can play a certain role in reducing water, with a water reducing rate of about 7.7%.
[0057] The emulsified paraffin ...
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