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Preparation device and method for nuclear track membrane

A technology for nuclear pore membranes and thin films, which is applied in the field of devices for preparing nuclear pore membranes. It can solve the problems of hindering etching, poor uniformity and fluidity of etching solution, and uneven distribution, so as to improve uniformity and fluidity, and improve etching. The effect of uniformity and micropore distribution

Pending Publication Date: 2019-05-28
上海谷奇核孔膜科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, the disadvantages of the above-mentioned traditional preparation process are as follows: first, when etching by immersion, white flocs are produced due to the chemical reaction between the membrane and the etching solution, and these flocs are easy to stay on the surface of the membrane, making the final nuclei Porous film is difficult to clean
Second, the pore size of the nuclear pore membrane is small, which undoubtedly increases the technical difficulty, especially during the etching process, a large number of flocs will be formed, which will reduce the etching rate, hinder the etching, and cause insufficient convection between the inner wall of the channel and the outside world, thus Affected to continue etching
Therefore, the small pore etching of nuclear pore membranes is a big problem
Third, due to the poor uniformity and fluidity of the etching solution in the existing etching tank, the reaction between the etching solution and the membrane is insufficient, and the finally formed pore size is unevenly distributed on the nuclear pore membrane and the pore size is not uniform

Method used

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  • Preparation device and method for nuclear track membrane
  • Preparation device and method for nuclear track membrane
  • Preparation device and method for nuclear track membrane

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Effect test

Embodiment 1

[0047] see figure 1 and combine figure 2, The nuclear pore membrane preparation device in the first embodiment includes: a sealing structure, a transmission component and a spraying area 200 . The sealing structure here adopts the pressing part 300 . The conveying part is used for conveying the original film 400 to be etched. Here, before entering the preparation device of the nuclear pore membrane, the pristine thin film 400 may be irradiated with heavy ions by using, but not limited to, heavy ions provided by a high-energy accelerator. Here, the original film 400 can be an organic film or an inorganic film. The original film 400 requires a certain hardness to withstand heavy ion radiation. Preferably, PET, PC, PP, PI, mica sheet or glass sheet can be used. films of other materials. The heavy ions provided by the high energy accelerator can be Kr, Ar, Xe, Bi ions. The energy of ion irradiation can be 5~50MeV / u, and the implantation meter of irradiation can be 1×10 4 up...

Embodiment 2

[0069] The difference between the preparation device of the nuclear pore membrane of the present embodiment 2 and the preparation device of the nuclear pore membrane of the embodiment 1 is that the setting of the spray area and the setting of the sealing mechanism are different, so that the sealing method and the sealing release method of the original film are different. . In addition, there is no corrosion solution tank in the second embodiment.

[0070] Specifically, see Figure 5 with 6 , In the second embodiment, the spray area 200 is provided with a vacuum adsorption part 700 and a sealing mechanism; the surface of the vacuum adsorption part 700 is provided with a plurality of suction holes. Specifically, the sealing mechanism is jointly composed of a vacuum adsorption component 700 and a flexible shielding component 301 . The joint sealing process between the two will be described in detail later. At the same time, the vacuum suction component 700 is also used to abs...

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Abstract

The invention provides a preparation device and method for a nuclear track membrane. According to the preparation device and method, an original thin film with a latent track subjected to the heavy-ion irradiation is conveyed to the relative position of a spraying component by utilizing a transmission component, spraying and etching are carried out on the surface to be etched of the original thinfilm with the latent track by utilizing the spraying component, etching liquid is sprayed on the surface to be etched of the original thin film, so that the latent track is etched into pores, and therefore the nuclear track membrane is formed. The preparation device and method have the advantages that the target pore diameter is formed on the original thin film by using a spraying mode, and therefore the uniformity and the fluidity of the etching liquid are improved, the etching uniformity is effectively improved, and finally, the nuclear track membrane which is uniform in micropore distribution and uniform in pore diameter can be obtained.

Description

technical field [0001] The invention relates to the technical field of filter membrane manufacturing, in particular to a device and method for preparing a nuclear pore membrane. Background technique [0002] The nuclear pore membrane is a sieving filter membrane, which has the advantages of regular pore shape, controllable and uniform pore size. At present, nuclear pore membranes are mainly used in medical filtration membranes, anti-counterfeiting, battery separators, biological detection membranes, water filtration, air filtration and other fields. [0003] The existing nuclear pore membrane preparation process includes two processes of irradiation and etching. The traditional etching process mainly uses the immersion of the nuclear pore membrane into the etching solution, and controls the etched pore size by controlling the etching time. [0004] However, the disadvantages of the above-mentioned traditional preparation process are as follows: first, when etching by immer...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/22B01D61/00B01D67/00C02F1/44H01M2/14H01M2/16H01M50/403
CPCY02E60/10
Inventor 王建中吕晓莉
Owner 上海谷奇核孔膜科技股份有限公司
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