Feather-like polyester fiber and preparation method thereof
A yarn polyester and feather technology is applied in the field of imitation feather yarn polyester fiber and its preparation, which can solve the problems of high equipment requirements, slow degradation rate, poor dyeing performance, etc., and achieve the effect of improving the interaction force
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Embodiment 1
[0055] A preparation method of feather-like polyester fiber, the steps are as follows:
[0056] (1) prepare modified polyester;
[0057] (1.1) Esterification reaction;
[0058]Make a slurry of terephthalic acid, ethylene glycol, dimethylsilanediol and 2,2-difluoro-1,3-malonic acid, add antimony trioxide, titanium dioxide and triphenyl phosphate and mix well , carry out the esterification reaction under pressure in a nitrogen atmosphere, the pressurized pressure is 0.3 MPa, the temperature of the esterification reaction is 250 ° C, when the amount of water distilled in the esterification reaction reaches 90.1% of the theoretical value, it is the end of the esterification reaction , the molar ratio of terephthalic acid to ethylene glycol is 1:1.2, the sum of the added amount of dimethylsilanediol and 2,2-difluoro-1,3-malonic acid is the added amount of terephthalic acid 3.2mol%, the molar ratio of dimethylsilanediol to 2,2-difluoro-1,3-malonic acid is 3:1.5, and the addition a...
Embodiment 2
[0076] A preparation method of feather-like polyester fiber, the steps are as follows:
[0077] (1) prepare modified polyester;
[0078] (1.1) Esterification reaction;
[0079] Make a slurry of terephthalic acid, ethylene glycol, dimethylsilanediol and 2,2-difluoro-1,4-butanedioic acid, add antimony ethylene glycol, titanium dioxide and trimethyl phosphate and mix well , the esterification reaction is carried out under normal pressure in a nitrogen atmosphere, the temperature of the esterification reaction is 260 ° C, when the amount of water distilled in the esterification reaction reaches 95% of the theoretical value, it is the end of the esterification reaction, and terephthalic acid The molar ratio with ethylene glycol is 1:2.0, the sum of the added amount of dimethylsilanediol and 2,2-difluoro-1,4-butanedioic acid is 5.0mol% of the added amount of terephthalic acid, two The molar ratio of methylsilanediol to 2,2-difluoro-1,4-butanedioic acid is 3:2, and the addition amo...
Embodiment 3
[0090] A preparation method of feather-like polyester fiber, the steps are as follows:
[0091] (1) prepare modified polyester;
[0092] (1.1) Esterification reaction;
[0093]Make a slurry of terephthalic acid, ethylene glycol, dimethylsilanediol and 2,2-difluoro-1,5-pentanedioic acid, add antimony acetate, titanium dioxide and trimethyl phosphite and mix evenly, The esterification reaction is carried out under pressure in a nitrogen atmosphere, the pressurized pressure is 0.2 MPa, and the temperature of the esterification reaction is 255 ° C. When the amount of water distilled in the esterification reaction reaches 92% of the theoretical value, it is the end point of the esterification reaction. The molar ratio of terephthalic acid to ethylene glycol is 1:1.6, the sum of the added amount of dimethylsilanediol and 2,2-difluoro-1,5-pentanedioic acid is 3.4 of the added amount of terephthalic acid mol%, the molar ratio of dimethylsilanediol to 2,2-difluoro-1,5-pentanedioic ac...
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