Tea polyphenol-containing carrageenan-based edible anti-oxidation membrane and preparation method thereof
An anti-oxidative film and tea polyphenol technology, applied in the field of food packaging, can solve the problems such as troublesome removal of packaging, difficult decomposition, waste, etc., and achieve the effects of broad market prospects, alleviation of environmental pollution, and improvement of high heat.
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Embodiment 1
[0049] According to the formula of 2%: 1.5%: 0.04%: 2%, k-carrageenan, sodium alginate, tea polyphenols, glycerin, etc. were weighed for later use. Dissolve κ-carrageenan in hot water at 90°C, heat and stir for 30 minutes, add glycerin; add tea polyphenols and sodium alginate fully dissolved in warm water at 40°C, and continue heating and stirring for 1 hour. After the prepared mixed solution was defoamed by an ultrasonic machine for 3 minutes, about 15 mL of the solution was poured into a clean glass dish of 5 cm*5 cm. After allowing the film to roughly form in the oven, soak in a low-concentration calcium chloride solution for 10 minutes, discarding excess liquid. Finally, the film was dried in an oven at 60°C until it was completely dry.
[0050] In terms of the performance of the film, the thickness of the prepared edible film was measured to be 70mm, and the water permeability was 0.810×10 -4 kg·mm(k·Pa·h·m 2 ), the oxygen permeability rate is 0.750×10 -14 cm 3 cm / (s...
Embodiment 2
[0052] According to the formula of 1%: 1%: 0.04%: 1%, k-carrageenan, sodium alginate, tea polyphenols, glycerin, etc. were weighed for later use. Dissolve κ-carrageenan in hot water at 90°C, heat and stir for 30 minutes, add glycerin; add tea polyphenols and sodium alginate fully dissolved in warm water at 40°C, and continue heating and stirring for 1 hour. After degassing the prepared mixed solution with an ultrasonic machine for 3 minutes, take about 15mL and pour it into a clean glass dish of 5cm*5cm. After allowing the film to roughly form in the oven, soak in a low-concentration calcium chloride solution for 10 minutes, discarding excess liquid. Finally, the film was dried in an oven at 60°C until it was completely dry.
[0053] In terms of the performance of the film, the thickness of the prepared edible film was measured to be 58mm, and the water permeability was 0.760×10 -4 kg·mm(k·Pa·h·m 2 ), the oxygen permeability rate is 0.680×10 -14 cm 3 cm / (s Pa), solubility...
Embodiment 3
[0055] According to the formula of 1%: 1.5%: 0.02%: 1%, k-carrageenan, sodium alginate, tea polyphenols, glycerin, etc. were weighed for later use. Dissolve carrageenan in hot water at 90°C and heat and stir for 30 minutes, then add glycerin; add tea polyphenols and sodium alginate fully dissolved in warm water at 40°C, and continue heating and stirring for 1 hour. After degassing the prepared mixed solution with an ultrasonic machine for 3 minutes, take about 15mL and pour it into a clean glass dish of 5cm*5cm. After allowing the film to roughly form in the oven, soak in a low-concentration calcium chloride solution for 10 minutes, discarding excess liquid. Finally, the film was dried in an oven at 60°C until it was completely dry.
[0056] In terms of film performance, the thickness of the prepared edible film was measured to be 50mm, and the water permeability was 0.800×10 -4 kg·mm(k·Pa·h·m 2 ), the oxygen permeability rate is 0.800×10 -14 cm 3 cm / (s Pa), solubility in...
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