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Color siloxane end-capped aqueous polyurethane hair dye and preparation method thereof,

A water-based polyurethane and siloxane technology, applied in hair care, pharmaceutical formulations, cosmetic preparations, etc., can solve discoloration and other problems, and achieve the effects of large molecular weight, good styling effect, and high gloss

Inactive Publication Date: 2019-05-07
安徽清彩科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Semi-permanent hair dyes also have disadvantages in that they can stain the skin when dyeing the hair, and the dye is washed out after 4 to 10 shampoos, and there will be discoloration in the later stage

Method used

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  • Color siloxane end-capped aqueous polyurethane hair dye and preparation method thereof,
  • Color siloxane end-capped aqueous polyurethane hair dye and preparation method thereof,
  • Color siloxane end-capped aqueous polyurethane hair dye and preparation method thereof,

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] The number average molecular weight M n2000 polypropylene glycol (PPG) was dehydrated at 110°C for 2 hours, then cooled to 50°C, 40 grams was added to a 500mL three-necked flask, and 24 grams of isophorone diisocyanate (IPDI) was added to stir and the temperature was raised to 80 After reacting at ℃ for 2 hours, add 2 grams of DYE1, 0.1 grams of dibutyltin dilaurate (DBTDL), 5 grams of dimethylol propionic acid (DMPA), 3 grams of 1,4-butanediol (BDO) and 0.5 grams of trihydroxy Methylpropane (TMP) and 30 grams of acetone were stirred at 70°C for 4 hours and then cooled to 40°C; after adding 5 grams of KH-540 and reacting for 10 minutes, 3.7 grams of triethylamine (TEA) and 20 grams of acetone were added. After reacting for 5 minutes, add 200 grams of water under high-speed stirring (1200 rpm), and after stirring for 30 minutes, transfer the reaction product to a rotary evaporator, and remove acetone at 45°C and 0.01MPa vacuum to obtain black silicon oxide Alkane-termin...

Embodiment 2

[0047] The number average molecular weight M n 2000 polypropylene glycol (PPG) was dehydrated at 110°C for 2 hours, then cooled to 50°C, 40 grams was added to a 500mL three-necked flask, and 24 grams of isophorone diisocyanate (IPDI) was added to stir and the temperature was raised to 80 After reacting at ℃ for 2 hours, add 2 grams of DYE2, 0.1 grams of dibutyltin dilaurate (DBTDL), 5 grams of dimethylol propionic acid (DMPA), 3 grams of 1,4-butanediol (BDO) and 1 gram of trihydroxy Methylpropane (TMP) and 30 grams of acetone were stirred at 70°C for 4 hours and then cooled to 40°C; after adding 5 grams of KH-792 and reacting for 30 minutes, 3.7 grams of triethylamine (TEA) and 20 grams of acetone were added. After reacting for 5 minutes, add 200 grams of water under high-speed stirring (1200 rpm), and after stirring for 30 minutes, transfer the reaction product to a rotary evaporator, and remove acetone at 45°C and 0.01MPa vacuum to obtain red silica Alkane modified water-ba...

Embodiment 3

[0051] The number average molecular weight M n 2000 polypropylene glycol (PPG) was dehydrated at 110°C for 2 hours, then cooled to 50°C, 40 grams was added to a 500mL three-necked flask, and 24 grams of isophorone diisocyanate (IPDI) was added to stir and the temperature was raised to 80 After reacting at ℃ for 2 hours, add 2 grams of DYE3, 0.1 grams of dibutyltin dilaurate (DBTDL), 5 grams of dimethylolpropionic acid (DMPA), 3 grams of 1,4-butanediol (BDO) and 1 gram of trihydroxy Methylpropane (TMP) and 30 grams of acetone were stirred at 70°C for 4 hours and then cooled to 40°C; after adding 5 grams of KH-602 and reacting for 40 minutes, 3.7 grams of triethylamine (TEA) and 20 grams of acetone were added. After reacting for 5 minutes, add 200 grams of water under high-speed stirring (1200 rpm), and after stirring for 30 minutes, transfer the reaction product to a rotary evaporator, and remove acetone at 45°C and 0.01MPa vacuum to obtain blue silicon Oxyalkylene modified wa...

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Abstract

The present invention discloses a color siloxane end-capped aqueous polyurethane hair dye and a preparation method thereof, and relates to the field of cosmetics. The hair dye comprises the followingcomponents in weight percentages: 10-80% of a color siloxane end-capped aqueous polyurethane emulsion, 0.1-1% of a thickener, 0.5-5.0% of sodium hyaluronate, 1.0-5.0% of amino acids, 1.0-5.0% of vitamin E, 0-5.0% of hydrolyzed proteins and the balance deionized water. The preparation method is as follows: the raw materials are taken in the amount according to the formula; and the raw materials areadded into a stirrer to be stirred evenly at a high speed of 800 rpm / min. The prepared color siloxane end-capped aqueous polyurethane hair dye is prepared by connecting dye molecules to a water-basedpolyurethane chain end-capped by a siloxane coupling agent through a chemical reaction, and the prepared color macromolecule hair dye has extremely excellent effects of adhesion and shaping, and at the same time has good shampoo resistance.

Description

technical field [0001] The invention belongs to the field of cosmetics, in particular to a colored silicone-terminated water-based polyurethane hair dye and a preparation method thereof. Background technique [0002] Hair dyeing has become a fashion. Young people can change the color of their hair according to their mood, and match their clothing and makeup to fully display their individuality. Walking on the street, you will find fashionable men and women using vivid and bright colors such as dark brown, linen, and wine red. Dress up a beautiful landscape, and currently hair dyes mainly contain three categories, namely permanent hair dyes, semi-permanent hair dyes and temporary hair dyes. [0003] Permanent hair dyes are mainly divided into oxidative hair dyes, inorganic hair dyes, and natural Chinese medicine hair dyes. [0004] Oxidative hair dye is the most widely used one at present, also known as permanent hair dye. Oxidative hair dye is mainly composed of color devel...

Claims

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Application Information

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IPC IPC(8): A61K8/87A61K8/44A61K8/64A61K8/67A61K8/73A61Q5/10C08G18/32
Inventor 李怡霞李军配陈军项羽曹苏毅吴祥松杨文东
Owner 安徽清彩科技有限公司
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