Complex compound of cross-linked polyvinylpyrrolidone and iodine and its preparation method and application
A technology for cross-linking polyvinylpyrrolidone and complexes, which is applied in the directions of active ingredients of iodine compounds, active ingredients of artificially synthesized polymeric materials, drug combinations, etc., can solve the problems of poor tissue exudation effect and poor stability, etc.
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Embodiment 1
[0050] Embodiment 1 prepares the complex compound of cross-linked polyvinylpyrrolidone and iodine
[0051] The present embodiment adopts the raw material of formula 1, the preparation method of the complex compound of cross-linked polyvinylpyrrolidone and iodine, comprises the following steps:
[0052] (1) In the reaction vessel with a temperature control device and a stirring device, add the cross-linked polyvinylpyrrolidone PVPP XL-10, refined iodine, alginate and catalyst in sequence, seal the reaction vessel, and stir the materials at normal temperature 60min to mix well, control the stirring speed to 50r / min.
[0053] (2) Set the reaction temperature to 80° C., stir, and control the stirring speed to 200 r / min. After the temperature rises to the temperature setting value, continue the heat preservation reaction for 24 hours.
[0054] (3), stop heating, lower the temperature of the material in the reactor, and discharge the material after the temperature of the material d...
Embodiment 2
[0056] Embodiment 2 prepares the complex compound of cross-linked polyvinylpyrrolidone and iodine
[0057] The present embodiment adopts the raw material of formula 2, the preparation method of the complex compound of cross-linked polyvinylpyrrolidone and iodine, comprises the following steps:
[0058] (1) In a reaction vessel with a temperature control device and a stirring device, add the cross-linked polyvinylpyrrolidone PVPPINF-10, refined iodine, alginate and catalyst in sequence, seal the reaction vessel, and stir the materials at room temperature for 50 minutes To mix evenly, control the stirring speed to 100r / min.
[0059] (2) Set the reaction temperature to 90°C, stir, and control the stirring speed to 300r / min. After the temperature rises to the temperature setting value, continue the heat preservation reaction for 20h.
[0060] (3), stop heating, lower the temperature of the material in the reactor, and discharge the material after the temperature of the material d...
Embodiment 3
[0062] Embodiment 3 prepares the complex compound of cross-linked polyvinylpyrrolidone and iodine
[0063] The present embodiment adopts the raw material of formula 3, the preparation method of the complex compound of cross-linked polyvinylpyrrolidone and iodine, comprises the following steps:
[0064] (1) In a reaction vessel with a temperature control device and a stirring device, sequentially add cross-linked polyvinylpyrrolidone PVPP XL, refined iodine, alginate and a catalyst in the prescribed amount, seal the reaction vessel, and stir the material for more than 40 minutes at normal temperature Mix evenly, and control the stirring speed to 150r / min.
[0065] (2) Set the reaction temperature to 100° C., stir, and control the stirring speed to 400 r / min. After the temperature rises to the temperature setting value, continue the heat preservation reaction for 18 hours.
[0066] (3), stop heating, lower the temperature of the material in the reactor, and discharge the materi...
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