Photosensitive resin composition and preparation method thereof
A technology of photosensitive resin and composition, which is applied in the direction of optomechanical equipment, photosensitive materials for optomechanical equipment, optics, etc., and can solve the problems of adhesion and solubility limitations, quality reduction and stability reduction in the development process, etc. Achieve low peeling difficulty, reduce development residue, and improve stability
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[0049] In a specific embodiment, the preparation method of the photosensitive resin composition comprises the following steps:
[0050] S1: Preparation of epoxy acrylate prepolymer
[0051] Weigh E-44 epoxy resin and acrylic acid at a weight ratio of 1:2, add 3-4% of onium salt of the total mass of the system as a catalyst, heat in a water bath, raise the temperature to 60-70°C, and stir for 3-5 hours to prepare a ring Oxyacrylate prepolymer;
[0052] S2: Preparation of modified styrene-acrylate copolymer
[0053] Weigh the reaction monomer according to the formula amount, stir it evenly and add it into the reaction kettle, add 2-3% of the total weight of the monomer azobisisoheptanonitrile initiator, keep the temperature of the water bath at 20-40°C, stir for 30-50min, Raise the temperature to 70-110°C and continue stirring for 3-5h to obtain a styrene-acrylate copolymer;
[0054] Add 2% toluenesulfonic acid of the total amount of monomers, then add 3.5-5 parts of (3S)-2,3...
Embodiment 1
[0073] The first aspect of Example 1 provides a photosensitive resin composition, comprising the following components in parts by weight: 21.5 parts of epoxy acrylate prepolymer, 56 parts of modified styrene-acrylate copolymer, alkali-soluble 18.9 parts of resin, 1.5 parts of photoinitiator and 1.2 parts of dye.
[0074] The modified styrene-acrylate copolymer is obtained by (3S)-2,3-dihydro-6-hydroxyl-3-benzofuran acetate modified styrene-acrylate copolymer; the styrene - The reaction monomer of the acrylate copolymer is styrene, methyl methacrylate, ethyl acrylate, and methacrylic acid is combined in a weight ratio of 1:3:4:3; the alkali-soluble resin is polyethylene glycol diacrylic acid 16 parts of esters, 0.3 parts of pentaerythritol triacrylate, 0.5 parts of 1,6-hexanediol diacrylate, 0.3 parts of 2-phenoxyethyl acrylate and 1.8 parts of triethylene glycol dimethacrylate; The photoinitiator is (3R,4R)-3-ethyl-4-[(E)-2-phenylvinyl]-2-azetidinone; the dye is 2-methylanthr...
Embodiment 2
[0086] The first aspect of Example 2 provides a photosensitive resin composition, comprising the following components in parts by weight: 20 parts of epoxy acrylate prepolymer, 50 parts of modified styrene-acrylate copolymer, alkali-soluble 13.5 parts of resin, 0.6 parts of photoinitiator and 1 part of dye.
[0087] The modified styrene-acrylate copolymer is obtained from (3S)-2,3-dihydro-6-hydroxyl-3-benzofuran acetate modified styrene-acrylate copolymer; the styrene - The reaction monomer of the acrylate copolymer is styrene, methyl methacrylate, ethyl acrylate, and methacrylic acid is combined according to a weight ratio of 1:3:4:3; the alkali-soluble resin is polyethylene glycol diacrylic acid 12 parts of ester, 0.1 part of pentaerythritol triacrylate, 0.1 part of 1,6-hexanediol diacrylate, 0.1 part of 2-phenoxyethyl acrylate and 1.2 parts of triethylene glycol dimethacrylate; The photoinitiator is (3R,4R)-3-ethyl-4-[(E)-2-phenylvinyl]-2-azetidinone; the dye is 2-methylan...
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