Environmentally-friendly low-fluorescence imitation asphalt plugging agent
A plugging agent, polyethylene glycol technology, applied in the field of oil drilling, can solve the problems of unsatisfactory anti-slump plugging, high fluorescence level, limited plugging effect, etc.
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Embodiment 1
[0031] Plugging agent a is composed of the following components in various mass percentages:
[0032] Polyamide wax powder 10%,
[0033] Oxidized Polyethylene Wax 20%,
[0034] PAC 5%,
[0035] Macrogol 20%,
[0036] Sodium dodecylbenzenesulfonate 2%,
[0037] Nano calcium carbonate 10% with a particle size of 40-70nm,
[0038] The balance is water.
[0039] Put the above components into the reaction kettle one by one according to the above arrangement order. After heating up to 120°C, stir at a constant temperature for 60 minutes. After all the components are completely mixed evenly, then cool down to normal temperature and pressure and stir at a high speed. Discharge after 30 minutes, dry at 120°C for 180 minutes, pulverize and granulate, and pass through a 200-mesh sieve.
Embodiment 2
[0041] The plugging agent b is composed of the following components in various mass percentages:
[0042] Polyamide wax powder 15%,
[0043] Oxidized Polyethylene Wax 25%,
[0044] PAC 8%,
[0045] Macrogol 25%,
[0046] Sodium dodecylbenzenesulfonate 3%,
[0047] Nano calcium carbonate 15% with a particle size of 40-70nm,
[0048] The balance is water.
[0049] The preparation method is the same as in Example 1, only the dosage of each component is replaced accordingly.
Embodiment 3
[0051] The plugging agent c is composed of the following components in various mass percentages:
[0052] Polyamide wax powder 20%,
[0053] Oxidized Polyethylene Wax 20%,
[0054] PAC 5%,
[0055] Macrogol 20%,
[0056] Sodium dodecylbenzenesulfonate 5%,
[0057] Nano calcium carbonate 15% with a particle size of 40-70nm,
[0058] The balance is water.
[0059] The preparation method is the same as in Example 1, only the dosage of each component is replaced accordingly.
[0060] Examples 1-3 According to the prepared environmentally friendly and easy-degradable imitation asphalt low-fluorescence plugging agent, the drilling fluid was prepared according to the following procedures and its performance was tested. For specific performance tests, refer to GB / T 16783.1-2006 Petroleum and Natural Gas Industry Drilling Fluid Field Test Part 1 : Water-based drilling fluid.
[0061] 1. Base slurry configuration program
[0062] 1) Take 400ml of fresh water, add 8g of bentonite...
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