Spinel Li-series ferrite materials for X-band to mm-wave band lock-in phase shifters
A ferrite material and millimeter wave technology, applied in the field of microwave technology and magnetic materials, can solve the problem of high remanence ratio, low coercivity, low coercivity, high remanence ratio, high Curie temperature and high power capacity and other problems, to achieve high remanence ratio, improvement of remanence ratio, and increase the effect of spin wave linewidth
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Embodiment 1
[0020] Spinel Li-based ferrite material for x-band to millimeter-wave band lock-in phase shifter, single-phase spinel structure, its composition chemical formula is,
[0021] Li 0.5(1-a+b-c-d-e) Zn a Mg e Ti b Cu c co d Bi n mn m Fe 0.5(5-a-3b-c-d-e)-m-n-δ o 4 ,
[0022] Where a=0.12, b=0.3, c=0.004, d=0.002, e=0.3, m=0.08, n=0.003, δ=0.02; calculate the required amount of each raw material according to the molecular formula. Use analytically pure Fe 2 o 3 , CuO, ZnO, Co 2 o 3 ,TiO 2 , MgO, MnCO 3 , Bi 2 o 3 , Li 2 CO 3 Raw materials, after treatment, calculate and weigh the corresponding weight according to the formula; once ball milled for 5 hours, mix evenly and then dry; pre-fire at 820°C, keep warm for 5 hours; then dry after the second ball mill for 5 hours, add 10% polyethylene Alcohol granulation, sintering at 980°C after molding, heat preservation for 5 hours; finally perform performance parameter test.
[0023] Apparent Density ρ of Materials Tes...
Embodiment 2
[0027] Spinel Li-based ferrite materials for lock-in phase shifters from x-band to millimeter-wave bands, single-phase spinel structure, and its composition chemical formula is:
[0028] Li 0.5(1-a+b-c-d-e) Zn a Mg e Ti b Cu c co d Bi n mn m Fe 0.5(5-a-3b-c-d-e)-m-n-δ o 4 ,
[0029] Where a=0.11, b=0.27, c=0.005, d=0.006, e=0.29, m=0.07, n=0.003, δ=0.04; calculate the required amount of each raw material according to the molecular formula. Use analytically pure Fe 2 o 3 , CuO, ZnO, Co 2 o 3 ,TiO 2 , MgO, MnCO 3 , Bi 2 o 3 , Li 2 CO 3 Raw materials, after treatment, calculate and weigh the corresponding weight according to the formula; once ball milled for 5 hours, mix evenly and then dry; pre-fire at 820°C, keep warm for 5 hours; then dry after the second ball mill for 5 hours, add 10% polyethylene Alcohol granulation, sintering at 980°C after molding, heat preservation for 5 hours; finally perform performance parameter test.
[0030] Apparent Density ρ of...
Embodiment 3
[0034] Spinel Li-based ferrite materials for lock-in phase shifters from x-band to millimeter-wave bands, single-phase spinel structure, and its composition chemical formula is:
[0035] Li 0.5(1-a+b-c-d-e) Zn a Mg e Ti b Cu c co d Bi n mn m Fe 0.5(5-a-3b-c-d-e)-m-n-δ o 4 ,
[0036] Where a=0.15, b=0.25, c=0.002, d=0.003, e=0.1, m=0.06, n=0.002, δ=0.06; calculate the required amount of each raw material according to the molecular formula. Use analytically pure Fe 2 o 3 , CuO, ZnO, TiO 2 , MnCO 3 ,Co 2 o 3 , Bi 2 o 3 , Li 2 CO 3 Raw materials, after treatment, calculate the corresponding weight according to the formula; once ball mill for 5 hours, mix evenly and then dry; pre-burn at 830°C, keep warm for 5 hours; then dry after the second ball mill for 5 hours, add 10% polyethylene Alcohol granulation, sintering at 990°C after molding, heat preservation for 5 hours; finally perform performance parameter test.
[0037] Measuring the Apparent Density ρ of Mat...
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