Waterborne polyurethane paint with high stability
A water-based polyurethane, stability technology, applied in the direction of polyurea/polyurethane coatings, coatings, etc., can solve the problems of application and development limitations, general storage stability, turbidity, etc.
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Embodiment 1
[0016] A waterborne polyurethane coating with good stability, which is made of the following components in parts by weight: modified waterborne polyurethane emulsion 98, polyethylene glycol 12, nano calcium carbonate 18, leveling agent 1.2, propylene glycol methyl ether acetate 2.5, Aluminum tripolyphosphate 2.8, pigment 1, deionized water 70.
[0017] Further, the preparation method of the modified waterborne polyurethane emulsion includes the following steps:
[0018] (1) Preparation of modifier: under inert atmosphere, mix unsaturated ester compounds, higher alcohols, sodium trimethylsiloxy, trichlorosilane, and chloroplatinic acid hexahydrate, and heat to 82°C at 1500r Stir for 20 minutes at speed per minute, then adjust the temperature to 88°C, keep the temperature in the water bath for 15 minutes, add initiator, stir evenly, reflux and stir for 3 hours, cool to room temperature naturally, and purify the reaction product to obtain the modifier; The molar ratio of the unsatura...
Embodiment 2
[0026] A waterborne polyurethane coating with good stability, which is made of the following components in parts by weight: modified waterborne polyurethane emulsion 105, polyethylene glycol 16, nano calcium carbonate 23, leveling agent 1.8, propylene glycol methyl ether acetate 3.6, Aluminum tripolyphosphate 3.5, pigment 2, deionized water 78.
[0027] Further, the preparation method of the modified waterborne polyurethane emulsion includes the following steps:
[0028] (1) Preparation of modifier: under inert atmosphere, mix unsaturated ester compounds, higher alcohols, sodium trimethylsiloxy, trichlorosilane, and chloroplatinic acid hexahydrate, and heat to 85°C at 1500r Stir for 30 min at speed per min, then adjust the temperature to 88°C, keep the temperature in the water bath for 15 min, add the initiator, stir evenly, reflux and stir for 4 hours, cool to room temperature naturally, and purify the reaction product to obtain the modifier; The molar ratio of the unsaturated es...
Embodiment 3
[0036] A waterborne polyurethane coating with good stability, which is made of the following components in parts by weight: modified waterborne polyurethane emulsion 102, polyethylene glycol 13, nano calcium carbonate 21, leveling agent 1.5, propylene glycol methyl ether acetate 2.8, Aluminum tripolyphosphate 3.1, pigment 1.2, deionized water 75.
[0037] Further, the preparation method of the modified waterborne polyurethane emulsion includes the following steps:
[0038] (1) Preparation of modifier: under inert atmosphere, mix unsaturated ester compounds, higher alcohols, sodium trimethylsiloxy, trichlorosilane, and chloroplatinic acid hexahydrate, and heat to 83°C at 1500r Stir for 25 min at speed per min, then adjust the temperature to 88°C, keep the temperature in a water bath for 15 min, add the initiator, stir evenly, stir at reflux for 3.4 hours, cool to room temperature naturally, and purify the reaction product to obtain the modifier; The molar ratio of the unsaturated e...
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