Tobacco flue-cured aromatic recycle tobacco leaf and preparation method thereof
A technology for reconstituting tobacco leaves and aroma type, which is applied in the directions of tobacco, tobacco preparation, application, etc., can solve the problems of increasing the irritation and miscellaneous gas of cigarettes, and the aroma of baking aroma is not prominent, and achieves improvement of baking aroma and smoking taste. , the effect of improving the quality of baking aroma, improving comfort and coordination
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Embodiment 1
[0035] Add 10 parts of flue-cured Zimbabwean tobacco, 1 part of Greek oriental tobacco, 5 parts of Sichuan sun-cured red tobacco, 100 parts of ethylene glycol, and 0.01 part of ferric chloride-ethylenediaminetetraacetic acid compound (molar ratio 1:3) Stir the round-bottomed flask, connect the mouth of the flask with a condenser to reflux, then put it into an oil bath and heat to 150°C, and react for 3 hours. Add 200 parts of petroleum ether to the above reaction product, ultrasonically extract for 60 minutes, then shake and extract for 60 minutes, then carry out centrifugation for 15 minutes, take the upper layer liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the desired Roasted flavored materials.
[0036] Add the above roasted flavor material to the reconstituted tobacco leaf coating solution at a ratio of 1:100, then add 0.5 times the amount of baicalin in the roasted flavor material, stir at room tempe...
Embodiment 2
[0042] 30 parts each of Henan flue-cured tobacco and Yunnan flue-cured tobacco, 2 parts of Turkish oriental tobacco and 3 parts of Xinjiang oriental tobacco, tobacco powder of 25 parts each of Hunan sun-cured red tobacco and Guangdong sun-cured red tobacco, 250 parts of propylene glycol, zinc lactate-tartaric acid compound ( Molar ratio 1:5) 1 part was added to a round bottom flask, stirred, the flask mouth was connected to a condenser tube to reflux, then put into an oil bath and heated to 250°C, and reacted for 0.5h. Add 2000 parts of n-hexane and chloroform to the above reaction product, ultrasonically extract for 10 minutes, then shake and extract for 10 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the obtained product. Roasted aroma materials required.
[0043]Add the above-mentioned roasted-flavor material to the reconstituted tobacco leaf coati...
Embodiment 3
[0048] Add 30 parts of American flue-cured tobacco, 2 parts of Baoshan oriental tobacco, 18 parts of Jilin sun-cured red tobacco, 200 parts of glycerin, and 0.1 part of zinc lactate-tartaric acid compound (molar ratio 1:5) into a round bottom flask, stir, and the flask A condenser was connected to the mouth to reflux, and then put into an oil bath and heated to 200°C, and reacted for 1h. Add 1000 parts of ethyl acetate to the above reaction product, ultrasonically extract for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, then carry out vacuum distillation to remove the solvent, and obtain the desired product. Roasted aroma materials.
[0049] Add the above roasted flavor material to the reconstituted tobacco leaf coating solution at a ratio of 1:50, then add 0.6 times the amount of baicalin in the roasted flavor material, stir at room temperature for 25 minutes to dissolve ...
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