A kind of preparation method of air-permeable and moisture-conducting fabric
A fabric and amino acid technology, applied in the field of fabrics, can solve the problems of poor hygroscopicity, difficulty, easy staining and staining of polyester, and achieve good washability, improved hygroscopicity, and improved moisture absorption and air permeability.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0044] A method for preparing a breathable and moisture-conducting fabric, specifically comprising the following steps:
[0045] S1, protection reaction of amino group
[0046] Add 200 mol of amino acid 1 and 400 mol of phthalic anhydride 2 into the reaction flask, add the solvent methylene chloride, and heat to reflux for 1.5 hours. After the reaction, remove the solvent by rotary evaporation to obtain the protected amino acid with the structure of formula 3. The yield is 96%; wherein, x in amino acid 1 is 1, and amino acid 1 is aspartic acid;
[0047]
[0048] S2, Esterification precondensation
[0049] Add 100 mol of terephthalic acid 4, 100 mol of protected amino acid 3, 400 mol of ethylene glycol 5 and 0.4 mol of catalyst aluminum acetate into a stainless steel reaction kettle, pass in nitrogen protection, and under a pressure of 0.2 MPa, heat up to 210°C for esterification , the oligomer 7 was obtained;
[0050]
[0051] S3, polycondensation reaction
[0052] The...
Embodiment 2
[0062] A method for preparing a breathable and moisture-conducting fabric, specifically comprising the following steps:
[0063] S1, protection reaction of amino group
[0064] Add 200 mol of amino acid 1 and 300 mol of phthalic anhydride 2 into the reaction flask, add the solvent methylene chloride, heat to reflux for 2 hours, and remove the solvent by rotary evaporation after the reaction, to obtain the protected amino acid with the structure of formula 3. The rate is 98%; wherein, x in amino acid 1 is 2, and amino acid 1 is glutamic acid;
[0065]
[0066] S2, Esterification precondensation
[0067]
[0068] Add 70 mol of terephthalic acid 4, 30 mol of protected amino acid 3, 180 mol of ethylene glycol 5 and 0.3 mol of catalyst aluminum acetate into a stainless steel reaction kettle, pass through nitrogen protection, and heat up to 225°C under a pressure of 0.2 MPa to perform esterification. , the oligomer 7 was obtained;
[0069] S3, polycondensation reaction
[...
Embodiment 3
[0080] A method for preparing a breathable and moisture-conducting fabric, specifically comprising the following steps:
[0081] S1, protection reaction of amino group
[0082] Add 200 mol of amino acid 1 and 440 mol of phthalic anhydride 2 into the reaction flask, add the solvent dichloromethane, heat to reflux for 2 hours, and remove the solvent by rotary evaporation after the reaction to obtain the protected amino acid with the structure of formula 3. The rate is 97%; wherein, x in amino acid 1 is 1, and amino acid 1 is aspartic acid;
[0083]
[0084] S2, Esterification precondensation
[0085] Add 60 mol of terephthalic acid 4, 40 mol of protected amino acid 3, 200 mol of ethylene glycol 5 and 0.25 mol of catalyst aluminum acetate into a stainless steel reaction kettle, pass in nitrogen protection, and under a pressure of 0.2 MPa, heat up to 220°C for esterification , the oligomer 7 was obtained;
[0086]
[0087] S3, polycondensation reaction
[0088] After the...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com