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Uniform mixing method of fe-cu-c-ceramic sic composite powder for powder metallurgy

A fe-cu-c-, powder metallurgy technology, applied in the field of powder metallurgy, can solve the problems of difficulty in retaining powder, irregular shape of iron powder, damage of shape and particle size distribution, and achieve the effect of promoting particle dispersion

Active Publication Date: 2020-06-02
CENT SOUTH UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The powder metallurgy process has its special requirements. The iron powder produced by the reduction method or the water atomization method has an irregular shape and a particle size of -100 mesh or -80 mesh (the average particle size is tens of microns). In order to keep the iron powder well pressed The shape and particle size distribution of iron powder should not be damaged much during the mixing process; it is necessary to maintain the shape and particle size distribution of iron powder and other raw materials. Or mechanical ball milling and other mixing methods, it is difficult to retain the shape of the original powder, and realize the uniform mixing of the original powder and the exogenous nanometer or submicron ceramic particles which are quite different from the iron base itself in physical properties

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] 0.2g of submicron SiC ceramic particles (volume 62.5mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and the volume is 56.25mm 3Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes, add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 2:1; speed 80rpm, ball milling time 30min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-type mixer (time 2h, speed 30rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particles Fe-2Cu-0.6C Compoun...

Embodiment 2

[0038] 0.4g submicron SiC ceramic particles (volume 125mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and a volume of 125mm 3 Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes; add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 2:1; speed 80rpm, ball milling time 30min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-shaped mixer (time 2h, rotation speed 30rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particle iron-based compos...

Embodiment 3

[0041] 0.8g submicron SiC ceramic particles (volume 250mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and a volume of 250mm 3 Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes; add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 4:1; speed 150rpm, ball milling time 60min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-type mixer (time 4h, rotation speed 40rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particle iron-based composi...

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Abstract

A uniform mixing method of Fe-Cu-C-ceramic SiC composite powder for powder metallurgy is aimed at submicron SiC ceramic particles without hydrogen bonds. The invention combines wet mixing and dry mixing techniques to evenly mix raw materials with large differences in physical properties (density, particle size, shape, etc.). Firstly, vibrate and disperse the submicron SiC ceramic particles and graphite, then add copper powder and the first iron powder with the same volume as the SiC ceramic particles to vibrate and disperse; Mix and add an appropriate amount of coupling agent and zinc stearate; the wet-mixed composite powder is vacuum-dried, sieved, and finally mixed with the remaining iron powder using a V-shaped mixer to prepare a uniformly mixed composite powder. The material mixing method of the present invention has simple process, convenient operation, combined with wet mixing and dry mixing techniques to implement step by step, and achieves uniform mixing of raw materials with large differences in physical properties (density, particle size, shape, etc.). Suitable for industrial applications.

Description

technical field [0001] The invention relates to a uniform mixing method of Fe-Cu-C-ceramic SiC composite powder for powder metallurgy, in particular to a uniform mixing method for adding submicron SiC ceramic powder to Fe-Cu-C powder for powder metallurgy . It belongs to the technical field of powder metallurgy. Background technique [0002] Powder metallurgy is a process technology that prepares the required products by preparing powder, mixing the powder evenly, pressing and molding, and sintering. [0003] When preparing composite materials by powder metallurgy technology, when the density, particle size and shape of the reinforcing particles and the matrix powder are similar, the mixing of the two can adopt the conventional method. For example, the invention patent application with the publication number CN 107686938A discloses an iron-based powder metallurgy friction material and its preparation method. It mixes iron-based powder and organic carbon source powder with ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F1/00B22F9/04
CPCB22F9/04B22F2009/042B22F2009/043B22F1/10
Inventor 李松林何勤求李普明袁勇于永亮仇朋
Owner CENT SOUTH UNIV
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