Uniform mixing method of fe-cu-c-ceramic sic composite powder for powder metallurgy
A fe-cu-c-, powder metallurgy technology, applied in the field of powder metallurgy, can solve the problems of difficulty in retaining powder, irregular shape of iron powder, damage of shape and particle size distribution, and achieve the effect of promoting particle dispersion
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Embodiment 1
[0035] 0.2g of submicron SiC ceramic particles (volume 62.5mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and the volume is 56.25mm 3Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes, add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 2:1; speed 80rpm, ball milling time 30min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-type mixer (time 2h, speed 30rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particles Fe-2Cu-0.6C Compoun...
Embodiment 2
[0038] 0.4g submicron SiC ceramic particles (volume 125mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and a volume of 125mm 3 Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes; add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 2:1; speed 80rpm, ball milling time 30min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-shaped mixer (time 2h, rotation speed 30rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particle iron-based compos...
Embodiment 3
[0041] 0.8g submicron SiC ceramic particles (volume 250mm 3 ) and graphite 0.6g into a cylindrical box, vibrate and disperse for 15min; add 2g of copper powder and a volume of 250mm 3 Put the iron powder into the cylindrical box, vibrate and disperse again for 5 minutes; add the vibration-dispersed powder into the ball mill jar, and add absolute ethanol and zinc stearate containing silane coupling agent KH-550, powder quality: ethanol solution Volume = 100g: 15ml, wet ball milling with low speed and low ball-to-material ratio (stainless steel ball diameter 5mm, ball-to-material mass ratio 4:1; speed 150rpm, ball milling time 60min); the powder after wet ball milling is vacuum-dried and passed through 45 mesh After sieving, the pre-composite powder is obtained, and the remaining iron powder is added to the pre-composite powder, mixed with a V-type mixer (time 4h, rotation speed 40rpm), and taken out to obtain uniformly dispersed submicron SiC ceramic particle iron-based composi...
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