Nano SiO2 modified PTFE needle blend filter material and preparation thereof and application thereof
A nano-modified technology, which is applied in the field of nano-SiO2 modified PTFE needle-punched blended filter material and its preparation, can solve the problems of poor filtering effect and achieve the effect of simple process, small size and high specific resistance
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Embodiment 1
[0044] (1) Hydrophobic nano-SiO 2 Particles and PTFE resin are mixed according to the mass ratio of 2:100, wherein, nano-SiO 2 The particle size is 20nm, put the prepared mixture into the mixer and stir at a constant speed for 3 hours to obtain the mixture 1; mix the mixture 1 and aviation kerosene according to the mass ratio of 100:20, and stir evenly in the mixer for 3 hours Hours, the mixture 2 was obtained, and then the uniform mixture 2 was left to stand at 50°C for 72 hours;
[0045] (2) Carry out pre-compression forming with the compacting machine of the mixture 2 that has been left still, the pressure is 4Mpa, and the pressing temperature is 25°C to make a columnar pre-compression molding body; then the pre-compression molding body is further pushed with a pusher Pressing, the pushing pressure is 4Mpa, and the pushing temperature is 160°C to make a rod-shaped extruded body; then the rod-shaped extruded body is pressed into a base belt with a calender, the calendering ...
Embodiment 2
[0052] According to step in embodiment 1, in step (1), hydrophobic nano-SiO 2 Particles and PTFE resin are mixed according to the mass ratio of 3:100, and the standing time is 96 hours. In step (2), the pre-compression molding pressure is 5Mpa, the pushing pressure is 6Mpa, the pushing temperature is 180 ° C, and the calendering temperature is 42°C, and the rest are the same as in Example 1 to obtain a single-layer nano-SiO 2 Modified PTFE needle-punched blend filter material, followed by monolayer nano-SiO 2 Three-layer lamination of modified PTFE needle-punched blended filter material to produce multi-layer composite nano-SiO 2 Modified PTFE needle-punched blend filter material.
[0053] Tested by optical contact angle measuring instrument, the nano-SiO 2 The contact angle of the modified PTFE needle-punched blended filter material is 146.8°, tested by the TSI 8130 filter tester, under the condition of a flow rate of 5.33cm / s, the multilayer composite nano-SiO 2 The filt...
Embodiment 3
[0055] According to step in embodiment 1, in step (1), hydrophobic nano-SiO 2 Granules and PTFE resin are mixed according to the mass ratio of 1:100, nano-SiO 2 The particle size is 50nm, the pre-compression molding pressure is 5Mpa in step (2), the pushing pressure is 6Mpa, the pushing temperature is 170°C, the calendering temperature is 45°C, the calendering line speed is 12m / min, and drying in step (3) The temperature is 310°C, the sintering temperature is 420°C, the drawing temperature is 380°C, the heat setting temperature in step (4) is 230°C, and the rest are the same as in Example 1 to obtain nano-SiO 2 Modified PTFE needle-punched blend filter material.
[0056] Tested by optical contact angle measuring instrument, the nano-SiO 2 The contact angle of the modified PTFE needle-punched blended filter material is 129.4°, tested by the TSI 8130 filtration tester, and the nano-SiO 2 The filtration efficiency of the modified PTFE needle-punched blended filter material for...
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