Sterilizing agent for vehicles and preparation method of sterilizing agent
A bactericide and vehicle technology, applied in the field of auto parts, can solve problems such as inability to effectively solve bacterial infestation, difficult to remove bacteria, explosive growth of bacteria, etc., achieve excellent bactericidal effect, improve bacteriostatic efficiency, and large specific surface area. Effect
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[0015] The present invention provides a kind of preparation method of described vehicle fungicide, comprises the following steps:
[0016] (1) Mix organic silicate and organic titanate to obtain mixed solution A, mix hexadecyltrimethylammonium bromide in water, and then add dropwise to the mixed system under stirring Mix solution A, after the dropwise addition, add a pH regulator to adjust the pH of the system to 5.3-6.2, then seal the mixed system at 100-160°C for 1-4 hours, centrifugally wash and dry the product, and store at 300-550°C Calcined for 1-2 hours to obtain silicon-titanium photocatalyst;
[0017] (2) Under ultrasonic conditions in a water bath, add aminopolyethylene glycol to the aqueous solution of graphene oxide, then add 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and N -Hydroxysuccinimide, stirred and reacted for 30-120 minutes to obtain graphene oxide modified by aminopolyethylene glycol, and then added 4-amino-1,2,4-triazole and maleic anhy...
Embodiment 1
[0025] A bactericide for vehicles, made of the following parts by weight: 2.5 parts by weight of tetraethyl titanate, 8 parts by weight of tetrabutyl silicate, 10 parts by weight of cetyltrimethylammonium bromide, hydrochloric acid ( 2M) 5 parts by weight, silane coupling agent KH5502 parts by weight, 3 parts by weight of aminopolyethylene glycol, 10 parts by weight of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, 12 parts by weight of N-hydroxysuccinimide, 15 parts by weight of graphene oxide, and 5 parts by weight of 4-amino-1,2,4-triazole.
[0026] The preparation method of described vehicle fungicide, the steps are as follows:
[0027] (1) Mix tetraethyl titanate and tetrabutyl silicate uniformly to obtain a mixed solution A, mix cetyltrimethylammonium bromide in water uniformly, and then add it to the mixed system under stirring Add the mixed solution A dropwise, after the dropwise addition, add hydrochloric acid to adjust the pH of the system to 6.2, then...
Embodiment 2
[0031]A bactericide for vehicles, made of the following parts by weight: 3 parts by weight of tetraethyl titanate, 5 parts by weight of tetrabutyl silicate, 8 parts by weight of cetyltrimethylammonium bromide, hydrochloric acid ( 2M) 2 parts by weight, 1.5 parts by weight of silane coupling agent KH550, 5 parts by weight of aminopolyethylene glycol, 12 parts by weight of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride 12 parts by weight of N-hydroxysuccinimide, 18 parts by weight of graphene oxide, and 10 parts by weight of 4-amino-1,2,4-triazole.
[0032] The preparation method of described vehicle fungicide, the steps are as follows:
[0033] (1) Mix tetraethyl titanate and tetrabutyl silicate uniformly to obtain a mixed solution A, mix cetyltrimethylammonium bromide in water uniformly, and then add it to the mixed system under stirring Add the mixed solution A dropwise, after the dropwise addition, add hydrochloric acid to adjust the pH of the system to 5.5, th...
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