Preparation method of composite flavor enhancer for cigarettes and application thereof
A flavor enhancer and composite technology, which is applied in the field of preparation of composite tobacco flavor enhancers, to achieve good application prospects, reduce smoke irritation, large market prospects and application value
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Embodiment 1
[0030] A preparation method of a compound flavor enhancer for cigarettes, comprising the steps of:
[0031] Step 1. Take 100 g of the whole plant of Sage sage, add 500 g of 75% ethanol and ultrasonically treat it for 2 hours, then reflux at 90°C for 5 hours, collect the reflux extract, concentrate under reduced pressure, and obtain the Sage Sage extract;
[0032] Step 2: Take 50g of Gembis cauliflower and dry it, grind it into powder, treat it with 0.2mol / L sulfuric acid 200g at 125°C for 30min, adjust the pH to 5.0 with mixed lye, add 2.75g of Gemlike cauliflower-quality mixed enzyme solution, and stir Evenly, after enzymatic hydrolysis at 65°C for 48 hours, adjust the pH to 4.5 with 6mol / L hydrochloric acid solution, add 0.25g glucoamylase of the quality of Geliflower, stir evenly, and enzymolyze at 60°C for 24h to obtain Geliflower extract ;
[0033] The mixed lye is formed by mixing 6 mol / L sodium hydroxide solution and 0.5 mol / L calcium hydroxide solution in a volume rat...
Embodiment 2
[0041] A preparation method of a compound flavor enhancer for cigarettes, comprising the steps of:
[0042] Step 1: Take 100 g of the whole Sage plant, add 600 g of 75% ethanol to ultrasonic treatment for 2 hours, then reflux at 75°C for 7 hours, collect the reflux extract, concentrate under reduced pressure, and obtain the Sage extract;
[0043] Step 2: Take 50 g of Gembis cauliflower, dry it, grind it into powder, treat it with 0.2 mol / L sulfuric acid 300 g at 125°C for 30 minutes, adjust the pH to 5.5 with mixed lye, add 3.2 g of Gembis cauliflower-quality mixed enzyme solution, and stir Evenly, after enzymatic hydrolysis at 65°C for 24 hours, adjust the pH to 5 with 6mol / L hydrochloric acid solution, add 0.36g of glucoamylase of the quality of Geliflower, stir evenly, and enzymolyze at 60°C for 24h to obtain Geliflower extract ;
[0044] The mixed lye is formed by mixing 6 mol / L sodium hydroxide solution and 0.5 mol / L calcium hydroxide solution in a volume ratio of 9:1. ...
Embodiment 3
[0052] A preparation method of a compound flavor enhancer for cigarettes, comprising the steps of:
[0053] Step 1: Take 100 g of the whole Sage plant, add 1000 g of 75% ethanol to ultrasonic treatment for 2 hours, then reflux at 90°C for 7 hours, collect the refluxed extract, concentrate under reduced pressure, and obtain the Sage extract;
[0054] Step 2: Take 50g of agaric cauliflower, dry it, grind it into powder, treat it with 0.2mol / L sulfuric acid 200g at 125°C for 30min, adjust the pH to 5.5 with mixed lye, add 3.25g of agaric cauliflower-quality mixed enzyme solution, and stir Evenly, after enzymatic hydrolysis at 65°C for 24 hours, adjust the pH to 4.8 with 6mol / L hydrochloric acid solution, add 0.32g of glucoamylase of the quality of Geliflower, stir evenly, and enzymolyze at 60°C for 48h to obtain Geliflower extract ;
[0055] The mixed lye is formed by mixing 6 mol / L sodium hydroxide solution and 0.5 mol / L calcium hydroxide solution at a volume ratio of 10:1.
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