Liquid fuel and preparation method thereof
A liquid fuel and ionic liquid technology, applied in the chemical field, can solve the problems of large catalyst consumption and long isomerization reaction time, and achieve low cost, small consumption and environmental friendliness
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Embodiment 1
[0018] Put 100g bridged tetrahydrotricyclopentadiene raw material in a three-necked round bottom flask, then put the three-necked flask into an oil bath, and after reaching 50°C, add an ionic liquid accounting for 10mol% of bridged tetrahydrotricyclopentadiene (1-Butyl-3-methylimidazolium chloride / AlCl 3 , where AlCl 3 The mole fraction is 0.6), stirring continuously for 3h, standing for 10min after the reaction, and separating the product from the ionic liquid by decantation. The product was characterized by gas chromatographic analysis, and the content of pendant tetrahydrotricyclopentadiene in the product was 95.0 wt%.
Embodiment 2-10
[0020] The reaction process of embodiment 2-10 is the same as embodiment 1, and difference is that adjustment reaction condition comprises: reaction temperature, catalyst (type, proportion, consumption) and reaction time, see the table below. The ionic liquids in Examples 8-10 are used repeatedly.
[0021]
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