Synthesis and application of hyperbranched surfactant
A surfactant and hyperbranched technology, which is applied in the preparation of organic compounds, organic chemistry, chemical instruments and methods, etc., can solve the problems of less active groups and small surfactant emulsification
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[0024] Accurately weigh 3.0021.g (0.03mol) of succinic anhydride with an electronic balance, place it in a beaker with a capacity of 100 mL, and add 30 mL of N,N-dimethylacetamide (DMAc) into the beaker to fully dissolve it. Add 3.9957 g (0.03 mol) of diisopropanolamine (moisture-proof) to a three-necked flask with a capacity of 500 mL. The three-necked flask is stirred with magnetic force, filled with nitrogen and exhausted. Put the fully dissolved succinic anhydride in a constant pressure dropper with a capacity of 100 mL, then place the constant pressure dropper on a three-necked flask, open the cock, and complete the dropwise addition in about half an hour, then react for 8 hours to obtain AB 2 monomer.
[0025] to AB 2 Add 1.3417 g (0.01 mol) nuclear molecule trimethylolpropane to the monomer to fully dissolve it, and then add 0.067 g of catalyst (p-toluenesulfonic acid) into the three-necked flask. Put the three-neck flask in an oil bath to heat, install a water separa...
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