Hydration heat regulation composition, as well as preparation method and application thereof
A composition and heat of hydration technology, applied in the field of concrete admixtures, can solve the problems of reduced concrete strength, reduced concrete durability, poor effect, etc., and achieve the effects of reducing corrosion, reducing heating and cooling rates, and improving safety
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Embodiment 1
[0041] Embodiment 1, the preparation of cationic acrylic resin
[0042] A mix 9 parts of methyl methacrylate, 7 parts of hydroxyethyl acrylate, 7 parts of isooctyl acrylate and 2 parts of butyl acetate hair agent to obtain a mixture;
[0043] B Add 1 / 2 of the mixture obtained in step A into 11 parts of n-butanol and stir until dissolved, then raise the temperature to 118°C, after heating for 22 minutes, add the remaining mixture obtained in step A dropwise at a rate of 0.4g / min, drop After the addition, the temperature was raised to 120°C for 2 hours of heat preservation reaction to obtain a polymer, and n-butanol was recovered under reduced pressure;
[0044] C Add 26 parts of diisocyanate to the polymer obtained in step B, raise the temperature to 75°C, keep the temperature for 2 hours, then cool down to 48°C, add 26 parts of pentaerythritol, then add 0.03 parts of stannous octoate, heat up to 80°C, and keep the temperature for reaction 2h, the extended chain prepolymer was...
Embodiment 2
[0047] Embodiment 2, the preparation of modified diatomite
[0048] a. Dry diatomaceous earth, pass through a 100-mesh sieve to obtain fine powder, then add hydrochloric acid with a volume concentration of 8%, the solid-to-liquid ratio of the fine powder to hydrochloric acid is 1g:2mL, heat to 110°C for 3h, Cool, wash with water until neutral, and dry to obtain acidic diatomite powder;
[0049] b. dissolving xylitol in water and stirring until completely dissolved, then adding the acidic diatomite powder obtained in step a and stirring, the weight ratio of xylitol and acidic diatomite powder is 6:1, forming a uniform colloid shape, dried, ground, that is.
Embodiment 3
[0050] Embodiment 3, a kind of hydration heat regulating composition
[0051] The hydration heat regulating composition consists of the following components and parts by weight thereof:
[0052] 48 parts of cationic acrylic resins, 14 parts of amino resins, 5 parts of epoxy phosphoric acid esters, 8 parts of tartaric acid and 18 parts of modified diatomaceous earths; The modified diatomite described above is the modified diatomite prepared in Example 2.
[0053] Preparation:
[0054] S1 First take cationic acrylic resin, amino resin and epoxy phosphate and stir evenly to obtain a mixture;
[0055] S2 Stir tartaric acid and modified diatomaceous earth evenly, then add to the mixture obtained in step S1, mix evenly, granulate, pass through 10-60 meshes, and obtain.
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