A method for improving polysaccharide dissolution rate of Pseudostellariae compound recipe and its products
A technology of Pseudostellaria Pseudostellariae and dissolution rate, which is applied in the field of traditional Chinese medicine processing, can solve the problems of long heating time at high temperature, incomplete dissolution of polysaccharides, and unfavorable effective utilization of active ingredients, and achieve the effect of avoiding high temperature and high pressure time and improving dissolution rate
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Embodiment 1
[0021] Weigh 1kg Pseudostellariae Radix, 1.5kg Radix Astragali and 2kg Jujube, add 10 liters of water and soak for 8 hours; drain the water and freeze at -18°C, keep the soaking water for subsequent extraction process; ) thawing; the raw materials after thawing were placed in a stainless steel grid tray, placed in a ventilated place at a temperature of 40°C to evaporate excess water, and the moisture content was measured to be 30.65% in 4 hours. Put the stainless steel mesh disk in the air explosion tank, raise the temperature inside the tank to 80°C, raise the pressure inside the tank to 0.1MPa higher than the atmospheric pressure outside the tank and keep it for 8 minutes, then drop the pressure inside the tank to a vacuum state for 30 minutes, and cool down to 40°C, release the vacuum, spray 4.5×10 to the material 5 U cellulase and 2.25 x 10 5 U pectinase (enzyme dissolved in distilled water, acetic acid to adjust the pH value to 5), keep warm at 40°C for 4 hours; after th...
Embodiment 2
[0024] Weigh 1 kg of Radix Pseudostellariae, 1.5 kg of Radix Astragali and 2 kg of Pitted Jujube, add 7 liters of water and soak for 24 hours, drain the water and freeze at -18°C for 6 hours, take it out at room temperature (18-25°C) and thaw; the thawed Pseudostellariae Put it into a stainless steel mesh pan, and blow off excess water at 60°C. After 4 hours, when the actual measured moisture is 27.13%, transfer the stainless steel mesh pan to an air explosion tank, raise the temperature inside the tank to 100°C, and The internal pressure rises to 0.3MPa higher than the atmospheric pressure outside the tank, and keeps for 3 minutes; then the pressure in the tank is instantly reduced to a vacuum state and kept for 30 minutes, then the vacuum is released, the temperature is lowered to 30°C, and 2.25×10 5 U cellulase and 9.0 x 10 4 U pectinase, insulated at 30°C for 10 hours, after the end of the heat preservation, the temperature in the tank was raised to 50°C, vacuumized until ...
Embodiment 3
[0026] Weigh heterophylla, astragalus, and jujube according to the formula, and perform gas explosion-enzyme revival treatment according to the method described in Example 1 or 2. Add 15 liters of water to the processed material, extract at 85°C for 40 minutes, filter, add 8 liters of water to the filter residue and continue to extract for 40 minutes, filter, and combine the filtrates. The filtrate was concentrated under reduced pressure until the specific gravity reached 1.1, and then freeze-dried to obtain instant powder of Radix Pseudostellaria Astragalus and Jujube.
[0027] The instant powder can be added with auxiliary materials, and the granules can be made according to the conventional method.
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