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Preparation method and application of anti-blue-ray film

An anti-blue light and microsphere technology, which is applied in optics, optical components, instruments, etc., can solve the problems of high technical threshold and few involvements

Active Publication Date: 2018-05-25
南通纳科达聚氨酯科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The technical threshold involved in the production and preparation of polymer photonic crystals is relatively high.

Method used

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  • Preparation method and application of anti-blue-ray film
  • Preparation method and application of anti-blue-ray film
  • Preparation method and application of anti-blue-ray film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Step (1) preparation of blue light reflective film

[0030] Using a 1L oil-bath stirred tank, protected by high-purity nitrogen, pre-mix 500g deionized water, 100g styrene, 10g methyl methacrylate, 10g acrylic acid, 2.5g ammonium bicarbonate, 2g sodium dodecylbenzenesulfonate, Stir at 70°C for about 30 minutes, then add a mixed solution of 3g ammonium persulfate and deionized water, and react at 75°C for two hours; then slowly add 5g ethyl acrylate, 5g propyl methacrylate, 0.2g A mixture of sodium dodecylbenzenesulfonate, 0.2g potassium hydroxide, and 100g deionized water to form a buffer layer; finally add a mixture of 100g ethyl acrylate and 0.2g sodium dodecylbenzenesulfonate in 120 minutes , 100g of deionized water mixture, and then react at 90°C for 60 minutes to allow the organic monomers to fully react. The composite microspheres were obtained by breaking the emulsion with methanol and drying.

[0031] After the composite microspheres are subjected to hot press...

Embodiment 2

[0033] Step (1) preparation of visible light reflective film

[0034] Use a 1L oil-bath stirred tank, protected by high-purity nitrogen, pre-mix 500g deionized water, 100g methyl methacrylate, 10g acrylic acid, 2.5g ammonium bicarbonate, 1g sodium dodecylbenzenesulfonate, stir at 70°C About 30 minutes, then add a mixed solution of 3g ammonium persulfate and deionized water, react at 75°C for two hours; then slowly add 5g ethyl acrylate, 5g propyl methacrylate, 0.2g dodecyl over 60 minutes A mixture of sodium benzenesulfonate, 0.2g potassium hydroxide, and 100g deionized water to form a buffer layer; finally, add a mixture of 100g ethyl acrylate, 0.2g sodium dodecylbenzenesulfonate, and 100g deionized water for 120 minutes. Water mixture, then react at 90°C for 60 minutes to allow the organic monomers to fully react. The composite microspheres were obtained by breaking the emulsion with methanol and drying.

[0035] After the composite microspheres are subjected to 130°C and ...

Embodiment 3

[0037] Preparation of anti-blue light film

[0038] Use a 1L oil-bath stirred tank, protected by high-purity nitrogen, pre-mix 500g deionized water, 100g styrene, 10g methyl methacrylate, 10g acrylic acid, 2.5g ammonium bicarbonate, 0.1g sodium dodecylbenzenesulfonate , stirred at 70°C for about 30 minutes, then added a mixed solution of 3g ammonium persulfate and deionized water, and reacted at 75°C for two hours; then slowly added 5g ethyl acrylate, 5g propyl methacrylate, 0.2 The mixed solution of sodium dodecylbenzene sulfonate, 0.2g potassium hydroxide, and 100g deionized water form a buffer layer; finally add a mixture of 100g ethyl acrylate and 0.2g sodium dodecylbenzenesulfonate in 120 minutes Liquid, 100g deionized water mixed solution, and then reacted at 90°C for 60 minutes to allow the organic monomers to fully react. The composite microspheres were obtained by breaking the emulsion with methanol and drying.

[0039] The composite microspheres can be hot-pressed ...

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Abstract

The invention discloses a preparation method and application of an anti-blue-ray film. The method comprises the following steps: 1) preparing a composite microsphere having a core-shell structure; and2) carrying out mirror rolling or one-way hot-pressing on the prepared composite microsphere to obtain a function film having an anti-blue-ray effect. The composite microsphere having the core-shellstructure is formed by a core, a transition layer and a shell from the inside out in sequence. The core is made of a spherical material, which is uniform in size, and deviation of which is less than 10%. The size of the spherical material is in a submicron range, and specifically refers to microspheres in 150-200 nm, which has higher reflection for blue rays in 380-420 nm. The beneficial effects are that the method adopts a pure chemical process to endow the film with the characteristics of multiple functions, and especially in the optical property of the thin film, free regulation of the solar spectrum is realized, such as control of visible light and high barrier of near infrared; and the anti-blue-ray film can be widely applied to fields of buildings, cars, ships and electronics and thelike.

Description

technical field [0001] The invention relates to a preparation method and application of an anti-blue light film, belonging to the field of functional films. Background technique [0002] Photonic crystal material is a new type of optical material, which refers to the regular arrangement of regular materials to form an optical forbidden band. This optical forbidden band can realize high reflection of light waves of a certain wavelength, and then filter out our Unwanted light waves. [0003] Opal in nature is a natural photonic crystal material. Silicon oxide or other inorganic nano-microspheres form a regular close-packed structure inside opal through complex and long-term crustal movement. This regularly arranged structure can reflect the sun. The visible light in the light makes the natural opal stone have brilliant colors. Inspired by the structure of natural opal, researchers have prepared various artificial photonic crystals since the 1980s, among which composite photo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G02B5/08G02B1/00
CPCG02B1/005G02B5/0808
Inventor 肖琳周振平叶航
Owner 南通纳科达聚氨酯科技有限公司
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