Ultra-high-speed flywheel made of graphene fiber composite material, as well as preparation method and application of graphene fiber composite material
A graphene fiber and composite material technology, which can be used in the fields of fiber chemical characteristics, spinning solution preparation, chemical instruments and methods, etc., and can solve problems such as inability to be widely used
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Embodiment 1
[0119] Embodiment 1 prepares semi-coke lignin
[0120] 1. Crushing of wood raw materials
[0121] Get dry woody raw material poplar branch and pulverize into woody raw material powder (poplar branch powder), the particle diameter of poplar branch powder≤1cm;
[0122] In the specific embodiment of the present invention, woody raw materials are described with poplar branches as raw materials, and other woody raw materials are applicable to the present invention, for example, crop straw, waste paper, wooden furniture, wood, etc.
[0123] 2. The first acid hydrolysis treatment
[0124] The poplar branch powder is placed in the first reaction tank that is equipped with the phosphoric acid solution of 5% by mass percent concentration, and the poplar branch powder is mixed with the catalyst phosphoric acid solution, wherein the weight ratio of the poplar branch powder to the catalyst is 2-7: 100 (preferably 4:100); then close the reaction tank, and heat up (in the embodiment of the...
Embodiment 2
[0132] 1. Preparation of graphite
[0133] 1A. Accurately weigh semi-coke lignin (0.5kg) and place it in a high-temperature carbonization furnace, heat up until the temperature reaches and maintains 900°C, and carry out carbonization treatment under the condition that the temperature is maintained at 900°C to obtain carbon powder ( 0.301kg), wherein the heating rate of the carbonization treatment is 10°C / min, and the carbonization treatment time is 45min;
[0134] 1B. Place the prepared carbon powder in a graphitization furnace, heat up to a temperature of 2100°C and keep it at 2100°C, and then pass nitrogen gas into it for protection, and carry out graphitization treatment to obtain a synthetic Graphite (0.251kg), wherein the heating rate of graphitization treatment is 10°C / min, and the time of graphitization treatment is 12min
[0135] 2. Preparation of graphene oxide
[0136] 2A. Add the synthetic graphite (0.251kg) prepared in the step 1) that was accurately weighed into...
Embodiment 3
[0160] 1. Preparation of graphite
[0161] 1A. Accurately weigh semi-coke lignin (0.5kg) and place it in a high-temperature carbonization furnace, heat up until the temperature reaches and maintains 1000°C, and carry out carbonization treatment under the condition that the temperature is maintained at 1000°C to obtain carbon powder ( 0.301kg), wherein the heating rate of the carbonization treatment is 15°C / min, and the carbonization treatment time is 35min;
[0162] 1B. Place the prepared carbon powder in a graphitization furnace, heat up to a temperature of 2400°C and keep it at 2400°C, and then pass nitrogen gas into it for protection, and carry out graphitization treatment to obtain a synthetic Graphite (0.252kg), wherein the heating rate of the graphitization treatment is 15°C / min, and the graphitization treatment time is 10min.
[0163] 2. Preparation of graphene oxide
[0164] 2A. Add the synthetic graphite (0.252kg) prepared in the step 1) that was accurately weighed ...
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