Nanometer material modified fluorocarbon resin stone material waterproof paint and preparation method thereof
A technology of modifying fluorocarbon and nanomaterials, applied in coatings and other directions, can solve the problems of reduced protection life, long-term protection life cannot meet user requirements, insufficient wear resistance or scrub resistance of coatings, etc. The effect of improving the anti-seepage performance, reducing the maintenance cost of the stone, and improving the protection life and protection effect
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Embodiment 1
[0020] Preparation of two-dimensional hexagonal boron nitride nanosheets: first, 33.80 g of lithium tetraborate (Li 2 B 4 o 7 ), 39.00g of sodium azide (NaN 3 ) and 19.20g of 400-mesh metal magnesium powder (Mg) are ball-milled and placed in a 500mL stainless steel high-temperature reaction kettle, sealed and put into a muffle furnace, and heated to 500°C at a rate of 10°C / min. Keep warm for 18 hours, and cool down to room temperature naturally after the reaction is completed. Take out the product in the high-temperature reactor and wash it with absolute ethanol and deionized water for 4 times, then soak it in a hydrochloric acid solution with a volume ratio of 1:1 and stir for 4 hours. During this period, the concentration of hydrochloric acid should be monitored, and the hydrochloric acid solution should be replenished in time. After the reaction was complete, the product was filtered with suction and washed three times with absolute ethanol. Finally, the cleaned product...
Embodiment 2
[0029] Preparation of two-dimensional hexagonal boron nitride nanosheets: first, 33.80 g of lithium tetraborate (Li 2 B 4 o 7 )), 63.50g of sodium azide (NaN 3 ) and 32.86g of 400-mesh metal magnesium powder (Mg) are ball-milled and placed in a 500mL stainless steel high-temperature reaction kettle, sealed and put into a muffle furnace, and heated to 600°C at a rate of 5°C / min. Keep warm for 24 hours, and cool down to room temperature naturally after the reaction is completed. Take out the product in the high-temperature reactor and wash it with absolute ethanol and deionized water for 4 times, then soak it in a hydrochloric acid solution with a volume ratio of 1:1 and stir for 4 hours. During this period, the concentration of hydrochloric acid should be monitored, and the hydrochloric acid solution should be replenished in time. After the reaction was complete, the product was filtered with suction and washed three times with absolute ethanol. Finally, the cleaned product...
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