High-property water-based metal die-casting releasing agent, preparation method and application of high-property water-based metal die-casting releasing agent
A release agent and metal mold technology, applied in metal processing equipment, casting molding equipment, casting molds, etc., can solve problems such as difficult to ensure the residual amount of lubricating components, burrs, pores, etc., to facilitate automated production, solve porous problems, The effect of strong heat resistance at high temperature
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[0037] The preparation method of metal die-casting release agent of the present invention comprises the steps:
[0038]Mixing of the oil phase system: adding the functional organic composition and the nonionic surfactant to the multifunctional reactor, and stirring to form an oil phase system;
[0039] W / O water-in-oil: Stir at 1000r / min, and drop water into the oil phase system to form a water-in-oil system. The amount of water added accounts for 1 / 10 of the mass of the oil phase system. The water-in-water system undergoes phase transformation to form an O / W oil-in-water system. After the phase transformation, stop adding water to the oil phase system and continue stirring for 5-10 minutes;
[0040] O / W oil-in-water: continue to inject water into the oil-in-water system for 3-5 minutes, the amount of water injected is 1 / 3-1 / 2 of the oil phase system, and the speed is increased to 1500r / min to make oil-in-water O / W W pre-emulsion, the speed is increased to 600r / min, and the p...
Embodiment 1
[0044] Example 1 is a specific example of preparing a mold release agent suitable for aluminum alloy die-casting. As shown in the following table 1, 1.5phr high carbonized phenolic resin contained in this embodiment, 20.6phr high temperature resistant silicone oil, 10.0phr refined rapeseed oil, 10.0phr high viscosity mineral oil, 3.0phr Span-80, 2.0phr 1310 , 1.0phr AEO-3, 1.0phr triethanolamine, 0.03phr isothiazolinone, 0.01phr benzisothiazolone and 50.86phr solvent.
[0045] Concrete preparation process is as follows:
[0046] Add high-carbonized phenolic resin, high-temperature-resistant silicone oil, high-viscosity mineral oil, refined rapeseed oil, Span-80, AEO-3 and 1310 into the multifunctional reaction kettle, and heat and stir to form an oil phase system at the same time. Then stir at a speed of 1000r / min, and add water dropwise to the oil phase system, and the dropwise addition is completed in 20 minutes to form an oil-in-water system. Continue to inject water into...
Embodiment 2
[0049] Example 2 is a specific example of preparing a release agent suitable for aluminum alloy die-casting. As shown in the following table 1, 1.0phr high carbonized phenolic resin contained in this embodiment, 24.0phr high temperature resistant silicone oil, 10.0phr refined rapeseed oil, 7.5phr high viscosity mineral oil, 2.6phr Span-80, 2.0phr 1310 , 1.0phr AEO-3, 1.0phr triethanolamine, 0.03phr isothiazolinone, 0.01phr benzisothiazolone and 50.86phr solvent.
[0050] Concrete preparation process is as follows:
[0051] Add high-carbonized phenolic resin, high-temperature-resistant silicone oil, high-viscosity mineral oil, refined rapeseed oil, Span-80, AEO-3 and 1310 into the multifunctional reaction kettle, and heat and stir to form an oil phase system at the same time. Then stir at a speed of 1000r / min, and add water dropwise to the oil phase system, and the dropwise addition is completed in 20 minutes to form an oil-in-water system. Continue to inject water into the s...
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