Heat-conducting pouring sealant and preparation method thereof
A heat-conducting potting and heat-conducting filler technology, applied in the direction of adhesives, adhesive types, polyether adhesives, etc., can solve the problems of large amount of heat-conducting fillers, high cost, unsuitable for large-scale production, etc. Good thermal conductivity, the effect of improving long-term stability
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Embodiment 1
[0067] In this embodiment, the thermally conductive potting compound is composed of agent A and agent B at a mass ratio of 5:1, and the agent A includes the following components by weight:
[0068]
[0069] The thermally conductive filler is alumina treated with titanate surface.
[0070] The B agent comprises the following components by weight:
[0071]
[0072] The preparation method is as follows:
[0073] (1) Stir and mix 107 glue with a viscosity of 1500mPa·s and methyl silicone oil at a vacuum degree of -0.1MPa at a stirring speed of 15r / min for 10min;
[0074] (2) Add thermally conductive fillers to the mixture obtained in step (1), and stir and mix for 40 minutes under a vacuum condition of -0.1 MPa, at a stirring speed of 45 r / min, and cooling with cooling water;
[0075] (3) Add aluminum hydroxide to the mixture obtained in step (2), and stir and mix for 20 min at a stirring speed of 15 r / min under a vacuum condition of -0.1 MPa in a vacuum;
[0076] (4) Add...
Embodiment 2
[0079] In this embodiment, the thermally conductive potting compound is composed of agent A and agent B at a mass ratio of 5.5:1, and the agent A includes the following components by weight:
[0080]
[0081]
[0082] The thermally conductive filler is alumina treated with titanate surface.
[0083] The B agent comprises the following components by weight:
[0084]
[0085] The preparation method is as follows:
[0086] (1) Stir and mix 107 glue with a viscosity of 1000mPa·s and ethyl silicone oil at a vacuum condition of -0.09MPa at a stirring speed of 20r / min for 15min;
[0087] (2) Add a thermally conductive filler to the mixture obtained in step (1), and stir and mix for 30 minutes under a vacuum condition of -0.09 MPa at a stirring speed of 50 r / min and cooling with cooling water;
[0088] (3) Add aluminum hydroxide to the mixture obtained in step (2), and stir and mix for 25min at a stirring speed of 10r / min under a vacuum condition of -0.1MPa in a vacuum;
...
Embodiment 3
[0092] In this embodiment, the thermally conductive potting compound is composed of agent A and agent B at a mass ratio of 6:1, and the agent A includes the following components by weight:
[0093]
[0094]
[0095] The thermally conductive filler is aluminum oxide treated with aminosilane.
[0096] The B agent comprises the following components by weight:
[0097]
[0098] The preparation method is as follows:
[0099] (1) Stir and mix 107 glue with a viscosity of 2000mPa·s and methyl silicone oil for 10min at a stirring speed of 10r / min under a vacuum condition of -0.1MPa;
[0100] (2) Add thermally conductive fillers to the mixture obtained in step (1), and stir and mix for 35 minutes under a vacuum condition of -0.09 MPa at a stirring speed of 40 r / min and cooling with cooling water;
[0101] (3) Add aluminum hydroxide to the mixture obtained in step (2), and stir and mix for 25min at a stirring speed of 20r / min under a vacuum condition of -0.09MPa in a vacuum; ...
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