Hydrogenation method for coal tar combination bed and system used for coal tar combination bed hydrogenation
A technology of coal tar and combined bed, which is applied to the hydrogenation system of coal tar combined bed and the field of hydrogenation of coal tar combined bed, which can solve the problems of coke clogging the internal components of the reactor and the inability to operate stably for a long period, so as to improve the utilization rate and utilization value, prolonging the operation period of the device, and improving the effect of liquid yield
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Embodiment 1
[0131] Based on the total weight of the coal tar raw material, the dosage of the slurry bed catalyst is 1.0% by weight based on the active metal elements contained therein. After mixing the coal tar raw material in Table 1 with the aforementioned highly dispersed heterogeneous slurry bed catalyst, they enter the slurry bed hydrogenation reactor together with hydrogen for gentle hydrogenation treatment, and the outflow of the slurry bed hydrogenation reactor The product enters the first separation unit for gas-liquid separation, and water is separated, and the separated liquid hydrocarbon product enters the fractionation tower, and the distillation is cut into light distillate, middle distillate and heavy distillate. Taking the corresponding heavy fraction in the coal tar raw material entering the slurry bed hydrogenation reactor as a benchmark, the conversion rate of the heavy fraction is controlled to be 50%. 50% by weight of the heavy fraction cut out by the distillation tow...
Embodiment 2
[0140] Present embodiment adopts the method similar to embodiment 1 to carry out, and difference is:
[0141] Based on the total weight of the coal tar raw material, the dosage of the slurry bed catalyst is 1.5% by weight based on the active metal elements contained therein. The coal tar raw material is uniformly mixed with the aforementioned high-dispersion heterogeneous slurry-bed catalyst, and then enters the slurry-bed hydrogenation reactor together with hydrogen for mild hydrogenation treatment. Taking the corresponding heavy fraction in the coal tar raw material entering the slurry bed hydrogenation reactor as a benchmark, the conversion rate of the heavy fraction in the slurry bed hydrogenation reactor is controlled to 65%. 60% by weight of the heavy fraction cut out of the fractionation tower is thrown out of the device, and the rest of the heavy fraction is recycled back to the slurry bed hydrogenation reactor for further conversion. Other main operating conditions a...
Embodiment 3
[0149] Present embodiment adopts the method similar to embodiment 1 to carry out, and difference is:
[0150] Based on the total weight of the coal tar raw material, the dosage of the slurry bed catalyst is 0.15% by weight based on the active metal elements contained therein. The coal tar raw material is uniformly mixed with the aforementioned high-dispersion heterogeneous slurry-bed catalyst, and then enters the slurry-bed hydrogenation reactor together with hydrogen for mild hydrogenation treatment. Taking the corresponding heavy fraction in the coal tar raw material entering the slurry bed hydrogenation reactor as a benchmark, the conversion rate of the heavy fraction in the slurry bed hydrogenation reactor is controlled to be 35%. Wherein the heavy fraction of 40% by weight cut out by the first fractionation system is thrown out of the device to control the solid content in the slurry bed hydrogenation reactor and maintain the active stability of the catalyst in the slurry...
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