Dispersive dye microcapsule and preparation method thereof
A disperse dye and microcapsule technology, applied in the field of textile printing and dyeing, can solve the problems of low core-encapsulation rate, no mechanical strength and hardness, and increased cost of disperse dye microcapsules, and achieve low pollution, low manufacturing cost, and high core-encapsulation rate. Improved effect
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Embodiment 1
[0029] Embodiment 1, a kind of disperse dye microcapsule
[0030] The disperse dye microcapsule described in Example 1 of the present invention is made up of the following components by weight: the weight ratio of described disperse dye, wall material and dispersant is 1:5:1, and described wall material is made of polyurethane and bacterial fiber The element is composed at a weight ratio of 1:0.3, wherein the dispersant is composed of citric acid and calcium hydrogen phosphate at a weight ratio of 1:0.2.
[0031] Preparation:
[0032] A) Mix the disperse dye with an appropriate amount of distilled water, emulsify, stir for 10 minutes, add 1 / 3 of the wall material dropwise, raise the temperature to 50°C, keep warm for 1 hour, add the dispersant, stir for 5 minutes, cool down to room temperature, and perform single-layer wall building;
[0033] B) Continue to add the remaining wall material dropwise, raise the temperature to 60°C, keep it warm for 1 hour, then lower it to room ...
Embodiment 2
[0034] Embodiment 2, a kind of disperse dye microcapsule
[0035] The disperse dye microcapsules described in Example 2 of the present invention consist of the following components in parts by weight: the weight ratio of the disperse dye, wall material and dispersant is 1:6.5:1.3, and the wall material is made of polyurethane and bacterial fiber The element is composed at a weight ratio of 1:0.6, wherein the dispersant is composed of citric acid and calcium hydrogen phosphate at a weight ratio of 1:0.4.
[0036] Preparation:
[0037] A) Mix the disperse dye with an appropriate amount of distilled water, emulsify, stir for 15 minutes, add 1 / 3 of the wall material dropwise, raise the temperature to 60°C, keep warm for 2 hours, add the dispersant, and at the same time continue to pass the normal voltage current, stir for 8 minutes, and drop to At room temperature, perform single-layer wall construction and turn off the power;
[0038] B) Continue to add the remaining wall mater...
Embodiment 3
[0039] Embodiment 3, a kind of disperse dye microcapsule
[0040]The disperse dye microcapsules described in Example 3 of the present invention are made up of the following components in parts by weight: the weight ratio of the disperse dye, wall material and dispersant is 1:8:3, and the wall material is made of polyurethane and bacterial fiber The element is composed by a weight ratio of 1:0.9, wherein the dispersant is composed of citric acid and calcium hydrogen phosphate by a weight ratio of 1:0.6.
[0041] Preparation:
[0042] A) Mix the disperse dye with an appropriate amount of distilled water, emulsify, stir for 20 minutes, add 1 / 3 of the wall material dropwise, raise the temperature to 70°C, keep warm for 2 hours, add the dispersant, and at the same time continue to pass through the normal voltage current, stir for 12 minutes, and drop to At room temperature, perform single-layer wall construction and turn off the power;
[0043] B) Continue to add the remaining wa...
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