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Method for extracting plant brown pigment

A brown pigment and plant technology, applied in the field of edible brown pigment extraction, can solve the problems of separation and purification difficulties, large differences in organic solvents, complicated preparation steps, etc., and achieve the effect of improving extraction efficiency, increasing adsorption effect, and cheap and easy-to-obtain raw materials

Active Publication Date: 2018-12-21
HUAIYIN INSTITUTE OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the complex preparation steps, low extraction efficiency, large differences in the organic solvents used for pigment components of different polarities, and the existence of solvent toxicity, volatility, and corrosiveness, it is easy to cause environmental pollution and solvent residues in the extract.
[0005] The emergence of ionic liquids was once considered to be a good substitute for traditional organic solvents, but with the deepening of research, people gradually found that these solvents were in some irreconcilable contradictions in the process of use.
For example, ionic liquids generally have high viscosity, recovery and separation and purification of products are difficult; and the preparation process of most ionic liquids is not green, and their own separation and purification are difficult, water absorption is serious, and the preparation cost is high; traditional imidazole and pyridine ions The liquid is non-renewable, difficult to degrade, and has obvious toxicity, etc., which directly leads to difficulties in the industrial application of ionic liquids.

Method used

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  • Method for extracting plant brown pigment
  • Method for extracting plant brown pigment
  • Method for extracting plant brown pigment

Examples

Experimental program
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Effect test

Embodiment approach 1

[0028] This embodiment provides a method for extracting brown pigment in apple seed shells. Take 10 g of apple seed shells that have been dried in the shade and crushed through a 40-mesh sieve, and use the deep eutectic solvent choline chloride-glycerol (molar ratio 1:2, Water content 0%wt) is the extraction solvent, and the solid-liquid ratio is 1g: 30mL, the ultrasonic power is 100W, the electrostatic field strength is 4kV, and the extraction temperature is 50°C, and the brown pigment extraction solution is obtained; petroleum ether and ethyl acetate are respectively used Wash the extract solution with the mixed solution for 3 times to obtain the degreasing pigment extract solution; add 5 g of attapulgite-loaded chitosan cross-linked cyclodextrin complex to the above degreasing extract solution, shake on a shaking table at 30°C and 100 r / min for 4 hours , take the precipitate after centrifugation, ultrasonically wash 3 times with deionized water, and centrifuge to obtain the ...

Embodiment approach 2

[0040] This embodiment provides a method for extracting brown pigment from apple seed shells. Take 10 g of apple seed shell powder that has been dried in the shade and crushed through a 40-mesh sieve, and use a deep eutectic solvent to extract choline nitrate-acetic acid (molar ratio 2: 3, water content 15%wt) as the extraction solvent, under the conditions of solid-to-liquid ratio 1g: 10mL, ultrasonic power 300W, electrostatic field strength 5kV, extraction temperature 50°C, extract for 20min to obtain brown pigment extract; use petroleum ether and acetic acid respectively Wash the extract with ethyl ester mixture for 3 times to obtain the degreasing pigment extract; add 3 g of attapulgite-loaded chitosan cross-linked cyclodextrin complex to the above degreased extract, and shake at 30°C and 100r / min. The bed was shaken for 5 hours, and the precipitate was collected by centrifugation, ultrasonically washed 3 times with deionized water, and centrifuged to obtain the brown pigme...

Embodiment approach 3

[0043] This embodiment provides a method for extracting brown pigment in apple seed shells. Take 10 g of apple seed shells that have been dried in the shade and crushed through a 40-mesh sieve, and use the deep eutectic solvent choline chloride-lactic acid-acetic acid (molar ratio 1:2: 1, water content 30%wt) as the extraction solvent, under the conditions of solid-liquid ratio 1g: 20mL, ultrasonic power 400W, electrostatic field strength 9kV, extraction temperature 60°C, extract for 30min to obtain brown pigment extract; use petroleum ether and acetic acid respectively Wash the extract with ethyl ester mixture for 3 times to obtain the degreasing pigment extract; add 2 g of attapulgite-loaded chitosan cross-linked cyclodextrin complex to the above-mentioned degreased brown pigment extract, at 30°C, 100r / min Vibrate on a shaking table for 5 hours, centrifuge to take the precipitate, wash it with deionized water ultrasonically for 3 times, and centrifuge to obtain the brown pigm...

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Abstract

The invention relates to the field of edible pigments, and discloses a method for extracting brown pigment from plants. After the plant containing brown pigment is crushed, a deep eutectic solvent extract is used to extract the brown pigment extract; petroleum ether and ethyl acetate are added to the extract The mixed solution is degreased, and the attapulgite-loaded chitosan cross-linked cyclodextrin complex is added to the degreased extract to obtain the brown pigment complex adsorbed on the attapulgite-loaded chitosan cross-linked cyclodextrin complex Precipitate; dissolve and desorb the precipitate in an organic solvent, and centrifuge to obtain a brown pigment supernatant containing an organic solvent; pass the supernatant through a microporous membrane to obtain a brown pigment solution containing an organic solvent; remove the organic solvent in the brown pigment solution Solvent to obtain the target product brown pigment. The invention uses a deep eutectic solvent as an extraction solvent, which is green, environmentally friendly, and has a high extraction rate; the attapulgite-loaded chitosan cross-linked cyclodextrin complex is used to purify and separate the brown pigment, and the process is simple and the purification and separation efficiency is high.

Description

technical field [0001] The invention relates to the technical field of edible brown pigment extraction, in particular to a method for extracting plant brown pigment. Background technique [0002] Natural pigments are pigments that people obtain from natural animals, plants or microbial cell tissues through certain technical means. Compared with synthetic pigments, they are non-toxic and natural in color, and have gradually become a new trend in the development of the world today. Their development and application It has also become a major research hotspot. [0003] Plant husks and seed husks are the by-products left after plants are eaten or processed. The husks or seed husks that account for a certain proportion of the whole fruit are often used as waste, fertilizer or fuel, and have not been effectively developed and utilized, resulting in a waste of resources. waste. A large number of studies have shown that the shells of plant fruits are rich in natural pigments, whic...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B61/00C09B67/54C09B67/10
CPCC09B61/00C09B67/0096
Inventor 毕艳红王朝宇付瑞平赵祥杰赵希荣
Owner HUAIYIN INSTITUTE OF TECHNOLOGY
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