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Phosphocholine modified candy anticaking agent as well as preparation method and application thereof

A technology of phosphorylcholine and anti-caking agent, which is applied in the field of phosphorylcholine-modified candy anti-caking agent and its preparation, and can solve problems affecting the effect of anti-caking agent

Inactive Publication Date: 2017-10-27
WUHU FOMAN BIOPHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Although the existing anti-caking agents can meet the needs of general customers, after a long period of storage, the effect of the anti-caking agent will drop in a straight line, which will affect the effect of the anti-caking agent

Method used

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  • Phosphocholine modified candy anticaking agent as well as preparation method and application thereof
  • Phosphocholine modified candy anticaking agent as well as preparation method and application thereof

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preparation example Construction

[0014] The present invention also provides a preparation method of phosphorylcholine-modified candy anticaking agent, comprising:

[0015] 1) ball milling aluminum silicate, talcum powder, magnesium phosphate, magnesium carbonate, phosphorylcholine and glycerol tristearate to obtain the primary product;

[0016] 2) drying the initial product to obtain an intermediate product;

[0017] 3) Mixing the intermediate product with crystalline cellulose to prepare a phosphorylcholine-modified anticaking agent for candy.

[0018] In step 1) of the above-mentioned preparation method, the consumption of each material can be selected in a wide range, but in order to further improve the anti-caking agent and the stability of the anti-caking agent, preferably, in step 1), aluminum silicate, The weight ratio of talcum powder, magnesium phosphate, magnesium carbonate, phosphorylcholine and glycerol tristearate is 100:40-60:3-8:22-28:1-3:50-65.

[0019] In step 1) of the above-mentioned prep...

Embodiment 1

[0029] 1) Aluminum silicate (average particle size 0.3 μm), talc powder (average particle size 0.2 μm), magnesium phosphate (average particle size 0.4 μm), magnesium carbonate (average particle size 0.3 μm), phosphoric acid bile Alkali (average particle diameter is 3nm) and glycerol tristearate carry out ball milling according to the weight ratio of 100:50:5:26:2:55 (the number ratio of large ball and small ball is 2:1.6, and grinding ball and The mass ratio of the material is 10:1.5, the rotating speed is 1100rpm, and the ball milling time is 50min) to obtain the initial product;

[0030] 2) drying the initial product at 90°C for 30 hours to obtain an intermediate product;

[0031] 3) Stir the intermediate product and crystalline cellulose at a weight ratio of 1:0.3 at 25° C. and 18,000 rpm for 2 hours to prepare phosphorylcholine-modified candy anticaking agent A1.

Embodiment 2

[0033] 1) Aluminum silicate (average particle size 0.1 μm), talc powder (average particle size 0.1 μm), magnesium phosphate (average particle size 0.1 μm), magnesium carbonate (average particle size 0.1 μm), phosphoric acid bile Alkali (average particle size is 1nm) and glycerol tristearate carry out ball milling according to the weight ratio of 100:40:3:22:1:50 (the number ratio of large ball and small ball is 2:1.5, and grinding ball and The mass ratio of the material is 10:1, the rotating speed is 1000rpm, and the ball milling time is 40min) to obtain the initial product;

[0034] 2) drying the initial product at 80°C for 24 hours to obtain an intermediate product;

[0035] 3) Stir the intermediate product and crystalline cellulose at a weight ratio of 1:0.1 at 15° C. and 1500 rpm for 1 hour to prepare phosphorylcholine-modified candy anticaking agent A2.

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Abstract

The invention provides a phosphocholine modified candy anticaking agent as well as a preparation method and application thereof. The preparation method comprises the following steps of (1) performing ball milling on aluminum silicate, talcum powder, magnesium phosphate, magnesium carbonate, phosphocholine and glyceryl tristearate to obtain a primary product; (2) drying the primary product so as to obtain an intermediate product; (3) mixing the intermediate product with avicel cellulose to prepare the phosphocholine modified candy anticaking agent. The anticaking agent has excellent anticaking performance and stability on candies; further, the anticaking agent can be applied to candies. Meanwhile, the preparation method has the advantages of simple work procedures and easy obtaining of raw materials.

Description

technical field [0001] The invention relates to a candy anticaking agent, in particular to a candy anticaking agent modified by phosphorylcholine, a preparation method and application thereof. Background technique [0002] The main purpose and function of anti-caking agents are: substances added to granular and powdered foods to prevent the aggregation and agglomeration of granular or powdered foods, and keep them loose or free-flowing. Potassium ferrocyanide, sodium aluminosilicate, tricalcium phosphate, silicon dioxide, and microcrystalline cellulose are allowed to be used in our country. Potassium ferrocyanide is prohibited in foods with "green" marks, and in general foods Its addition limit is 0.01g / kg. [0003] Although the existing anti-caking agents can meet the needs of general customers, the effect of the anti-caking agents plummets after being placed for a long time, thereby affecting the effect of the anti-caking agents. Contents of the invention [0004] The ...

Claims

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Application Information

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IPC IPC(8): A23G3/36A23G3/42A23G3/40A23P10/43
CPCA23G3/36A23G3/362A23G3/40A23G3/42A23V2002/00A23P10/43A23V2200/208A23V2250/1628A23V2250/1564A23V2250/1576A23V2250/161A23V2250/1618A23V2250/1942A23V2250/51084A23V2300/10
Inventor 苏福男
Owner WUHU FOMAN BIOPHARMA CO LTD
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