Polyvinylidene fluoride anti-pollution membrane and preparation method thereof
A technology of polyvinylidene fluoride film and polyvinylidene fluoride, which is applied in the field of environmental functional film materials, can solve the problems of poor pollution resistance and insufficient modification degree of polyvinylidene fluoride, and achieve low requirements for preparation equipment and anti-pollution Strong ability and good filtration performance
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Embodiment 1
[0024] (1) Preparation of Tris-HCl buffer solution: Dissolve 0.1815 g of Tris-HCl in 300 mL of distilled water, and adjust the pH to 8.5 with hydrochloric acid to obtain a Tris-HCl buffer solution;
[0025] (2) Dopamine-modified PVDF powder: under continuous magnetic stirring at room temperature, quickly add 0.3g dopamine hydrochloride, 6.0g PVDF powder and 10mL absolute ethanol to the Tris-HCl buffer solution obtained in step (1), and magnetically stir at 25°C After 6-24 hours, filter, wash the obtained solid with deionized water, and then place the product in a vacuum dryer at 40°C to dry to constant weight, that is, dopamine-modified PVDF powder;
[0026] (3) disperse 6.0g of dopamine-modified polyvinylidene fluoride powder obtained in step (2), 0.4g of polyvinylpyrrolidone (PVP) in 13.2g of N,N-dimethylformamide (DMF) or N-formaldehyde In NMP or N, N-dimethylacetamide (DMAC), stir magnetically at 50-70°C for 2-6 hours to form a uniform casting solution. After vacuum degass...
Embodiment 2
[0029] (1) with embodiment 1;
[0030] (2) with embodiment 1;
[0031] (3) with embodiment 1;
[0032](4) Soak the dopamine-modified PVDF membrane obtained in step (3) in 100mL of 0.3mol / L H 3 BO 3 in aqueous solution for 2min, and then transferred to 110mL of newly prepared pH 3.87 ammonium fluotitanate and boric acid (0.1mol / L (NH 4 ) 2 TiF 6 +0.3mol / L H 3 BO 3 ) in a mixed aqueous solution at room temperature for 45 minutes, and the prepared membrane was fully washed in deionized water to obtain the PVDF anti-fouling membrane.
Embodiment 3
[0034] (1) with embodiment 1;
[0035] (2) with embodiment 1;
[0036] (3) with embodiment 1;
[0037] (4) Soak the dopamine-modified PVDF membrane obtained in step (3) in 100mL of 0.3mol / L H 3 BO 3 in aqueous solution for 2 min, and then transferred to 110 mL of freshly prepared pH 3.87 ammonium fluorotitanate and boric acid (0.1 mol / L (NH 4 ) 2 TiF 6 +0.3mol / L H 3 BO 3 ) in a mixed aqueous solution, continue to soak for 15 minutes at room temperature, and then fully wash the prepared membrane in deionized water to obtain the PVDF anti-fouling membrane.
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