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Adsorbing stuffing for treating aniline-containing wastewater and preparation method and application thereof

A kind of technology of aniline wastewater and adsorption filler, which is applied in water/sewage treatment, chemical instruments and methods, adsorption water/sewage treatment, etc. It can solve the problems of cumbersome treatment steps, unsuitable for industrial wastewater treatment, and unsuitable for large-scale industrial wastewater , to achieve the effect that the preparation method is simple and easy, and it is easy to elute and regenerate

Active Publication Date: 2017-07-14
微纯生物科技(广州)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, because the processing steps of this method are cumbersome, involving steps such as heating, pH adjustment, and flocculation, it is not suitable for the treatment of large quantities of industrial wastewater; the Chinese invention patent application with application number 201610095154. This method is a method for treating aniline wastewater. In this method, various strains are symbiotic and coordinated, and they are not antagonistic to each other. When added to the wastewater treatment system, it has a good degradation effect on aniline refractory compounds.
However, the regeneration of fungi is complicated and not suitable for the treatment of large quantities of industrial wastewater

Method used

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  • Adsorbing stuffing for treating aniline-containing wastewater and preparation method and application thereof
  • Adsorbing stuffing for treating aniline-containing wastewater and preparation method and application thereof
  • Adsorbing stuffing for treating aniline-containing wastewater and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Example 1: Preparation of adsorption packing for treating aniline-containing wastewater.

[0037] At room temperature, add deionized water (500mL), Triton X-100 (6.3g) and sodium dodecylsulfonate (0.7g) into a 1L three-necked flask, and stir for 30min to obtain a homogeneous aqueous phase solution.

[0038] At room temperature, methyl acrylate (80 g), styrene (10 g) and 4-aminostyrene (10 g) were added into a 500 mL Erlenmeyer flask and stirred evenly to obtain a colorless and transparent oil phase solution.

[0039] At room temperature, add azobisisobutyronitrile (0.2 g) to the above oil phase solution, stir to dissolve, then add it to the above water phase solution, and shear and stir (domestic S312-90 mechanical stirrer, stirring plate The diameter of rotation is 10 cm, and the stirring speed is 500 rpm), until a uniform and stable O / W emulsion (the average particle size of the oil phase droplets is about 300 μm) is obtained.

[0040] Raise the temperature of the a...

Embodiment 2

[0041] Example 2: Preparation of adsorption filler for treating aniline-containing wastewater.

[0042] Add deionized water (500mL), Tween-20 (6.5g) and sodium dodecylbenzenesulfonate (0.5g) into a 1L three-necked flask at room temperature, and stir for 30min to obtain a homogeneous aqueous phase solution .

[0043] At room temperature, ethyl acrylate (80 g), styrene (10 g) and 3-aminostyrene (10 g) were added into a 500 mL Erlenmeyer flask and stirred evenly to obtain a colorless and transparent oil phase solution.

[0044] At room temperature, add azobisisobutyronitrile (0.2 g) to the above oil phase solution, stir to dissolve, then add it to the above water phase solution, and shear and stir (domestic S312-90 mechanical stirrer, stirring plate The diameter of rotation is 10 cm, and the stirring speed is 300 rpm), until a uniform and stable O / W emulsion (the average particle size of the oil phase droplets is about 500 μm) is obtained.

[0045] Raise the temperature of the ...

Embodiment 3

[0046] Example 3: Preparation of adsorption packing for treating aniline-containing wastewater.

[0047] Add deionized water (500mL), Tween-20 (6.5g) and sodium dodecylbenzenesulfonate (0.5g) into a 1L three-necked flask at room temperature, and stir for 30min to obtain a homogeneous aqueous phase solution .

[0048] At room temperature, butyl acrylate (50 g), styrene (30 g) and 4-aminostyrene (20 g) were added into a 500 mL Erlenmeyer flask and stirred evenly to obtain a colorless and transparent oil phase solution.

[0049] At room temperature, add azobisisobutyronitrile (0.2 g) to the above oil phase solution, stir to dissolve, then add it to the above water phase solution, and shear and stir (domestic S312-90 mechanical stirrer, stirring plate The diameter of rotation is 10 cm, the stirring speed is 80 rpm), until a uniform and stable O / W emulsion (the average particle diameter of the oil phase droplets is about 1000 μm) is obtained.

[0050] Raise the temperature of the a...

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Abstract

The invention belongs to the technical field of wastewater treatment and relates to adsorbing stuffing for treating aniline-containing wastewater and a preparation method and an application thereof. In particular, the preparation comprises the following steps: 1) preparing a mixed solution of a surfactant and water as an aqueous phase; 2) preparing a mixed solution of acrylate, styrene and amino styrene as an oil phase; 3) preparing an O / W emulsion; and 4) performing free radical emulsion polymerization. The preparation method is simple and feasible. The grain size of the adsorbing stuffing prepared by the method is 200-2000[mu]m, and the adsorbing stuffing can effectively adsorb and enrich aniline in water, is easily eluted and generated and is suitable for industrial treatment of aniline-containing wastewater.

Description

technical field [0001] The invention belongs to the technical field of wastewater treatment, and relates to an adsorption filler for treating wastewater containing aniline, a preparation method thereof, and an application in treating wastewater containing aniline. Background technique [0002] Aniline is the most representative aromatic amine substance. It is a colorless oily liquid with aromatic odor. It is widely used in industries such as national defense, printing and dyeing, plastics, paint, pesticides and medicine. In addition, aniline is also a harmful substance that seriously pollutes the environment and endangers human health, and belongs to the three substances of "carcinogenic, teratogenic, and mutagenic". Due to the characteristics of long-term residue, bioaccumulation, and carcinogenicity, aniline is listed as 129 pollutants for priority control by the US EPA; at the same time, it is also included in the "China Environmental Priority Pollutants Blacklist" and is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/26B01J20/30C08F220/14C08F212/08C08F212/14C08F220/18C08F2/26C08F2/30C02F1/28C02F101/38
CPCB01J20/261C02F1/285C02F2101/38C08F2/26C08F2/30C08F220/14C08F220/18C08F220/1804C08F212/08C08F212/14
Inventor 黄晓马西飞刘钰姚旭
Owner 微纯生物科技(广州)有限公司
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