Preparation process of neptunium oxide target pellets
A preparation process, neptunium oxide technology, applied in the field of neptunium oxide target pellet preparation process, can solve the problems of complex process, high production cost, low loading capacity, etc., and achieve the goal of simple process flow, low cost and high neptunium utilization rate Effect
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Embodiment 1
[0019] (1) Neptunium oxide powder and magnesium oxide powder are taken as target pellet raw materials as required, wherein the quality of magnesium oxide powder accounts for 1% of the total mass of the two;
[0020] (2) In the neptunium oxide powder, take out the neptunium oxide powder equal to the mass of the magnesium oxide powder, mix the taken out neptunium oxide powder with the magnesium oxide powder in a three-dimensional motion mixer for 6 hours, and obtain the primary mixed powder ;
[0021] (3) Add the remaining neptunium oxide powder and stearic acid into the three-dimensional motion mixer, make it continue to mix with the aforementioned primary mixing powder for 3 hours, and obtain the mixed powder; wherein, the addition of stearic acid accounts for all neptunium oxide powder and oxidation 0.2% of the total mass of magnesium powder;
[0022] (4) In the glove box, a hydraulic press is used to cold-press the mixed powder with a pressure of 350 MPa, and the holding ti...
Embodiment 2
[0025] (1) Neptunium oxide powder and magnesium oxide powder are taken as target pellet raw materials as required, wherein the quality of magnesium oxide powder accounts for 5% of the total mass of the two;
[0026] (2) In the neptunium oxide powder, take out the neptunium oxide powder accounting for 0.5 times the mass of the magnesium oxide powder, mix the taken out neptunium oxide powder with the magnesium oxide powder in a three-dimensional motion mixer for 4 hours, and obtain the initial mixing powder;
[0027] (3) Add the remaining neptunium oxide powder and stearic acid into the three-dimensional motion mixer, make it continue to mix with the aforementioned primary mixing powder for 2 hours, and obtain the mixed powder; wherein, the addition of stearic acid accounts for all neptunium oxide powder and oxidation 0.4 of the total mass of magnesium powder;
[0028] (4) In the glove box, a hydraulic press is used to cold press the mixed powder with a pressure of 400 MPa, and...
Embodiment 3
[0031] (1) taking neptunium oxide powder and magnesium oxide powder as target piece raw material as required, wherein the quality of magnesium oxide powder accounts for 10% of the total mass of the two;
[0032] (2) In the neptunium oxide powder, take out the neptunium oxide powder accounting for 4 times the mass of the magnesium oxide powder, and mix the taken out neptunium oxide powder and the magnesium oxide powder in a three-dimensional motion mixer for 8 hours to obtain an initial mix powder;
[0033] (3) Add the remaining neptunium oxide powder and stearic acid into the three-dimensional motion mixer, make it continue to mix with the aforementioned primary mixing powder for 5 hours, and obtain the mixed powder; wherein, the addition of stearic acid accounts for all neptunium oxide powder and oxidation 0.6 of the total mass of magnesium powder;
[0034] (4) In the glove box, a hydraulic press is used to cold-press the mixed powder with a pressure of 600 MPa, and the hold...
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