PS [PAM-Ca-LS (polyacrylamide-calcium lignin sulfonate)] lignin gel type profile control agent and method for preparing same
A gel type, profile control agent technology, applied in chemical instruments and methods, drilling compositions and other directions, can solve the problems of short profile control validity period, low plugging efficiency, high initial viscosity, and the gel time can be adjusted. , The effect of high blocking efficiency and low product cost
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Embodiment 1
[0012] First add 471.0g water to the container, then add 10g gelling agent calcium lignosulfonate, 2.0g colloidal stabilizer thiourea, 2.5g reducing agent anhydrous sodium sulfite, 2.0g chelating agent tetrasodium edetate, After circulating and stirring for half an hour at normal temperature and pressure, slowly sprinkle 4.0g of high molecular polymer polyacrylamide, circulate and stir for 2 hours, and let it stand for 8 hours to become lignin gel type profile control agent A; at the same time, 4.0g Dissolve the cross-linking agent Sodium Red Alum completely in another container with 4.0g of water to form the lignin gel type profile control agent B; add 0.5g retarder sodium citrate to Agent A before injecting, and then add Agent B to it , stir to get 500g product. The apparent viscosity of the base fluid was tested with a rotational viscometer to be 150.0 mPa·s. Then the product was put into an oven at 50°C for reaction, and the gelation time was tested for 5 hours; the gelat...
Embodiment 2
[0014] First add 452.5g water in the container, then add 20g gelling agent calcium lignosulfonate, 2.5g colloidal stabilizer thiourea, 2.5g reducing agent anhydrous sodium sulfite, 2.0g chelating agent tetrasodium edetate, After circulating and stirring at normal temperature and pressure for half an hour, slowly sprinkle 6.0g of high molecular polymer polyacrylamide, circulate and stir for 2 hours, and let it stand for 8 hours to become lignin gel type profile control agent A; at the same time, 6.0g Dissolve the cross-linking agent sodium red alum completely in another container with 6.0g of water, and it is the lignin gel type profile control agent B agent; add 2.5g retarder sodium citrate to agent A before injection, and then add agent B to it , stir to get 500g product. The apparent viscosity of the base fluid was measured with a rotational viscometer to be 230.0 mPa·s. Then put the product into an oven at 50°C for reaction, and test the gelation time for 24 hours. The ge...
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