Preparation method of GaN-based semiconductor used for LED
A gallium nitride-based semiconductor technology, applied in the field of gallium nitride-based semiconductor preparation, can solve problems such as poor anti-static breakdown capability, reduced diode performance, and reduced internal quantum efficiency, so as to reduce internal leakage and improve reverse performance. Voltage, effect of reducing operating speed
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Embodiment 1
[0035] h 2Purify the substrate at high temperature in the environment; H at 1000°C 2 Under the atmosphere, feed 100L / min of H 2 , keep the reaction chamber pressure at 100mbar, and process the substrate for 8min.
[0036] The epitaxial wafer includes a multi-quantum well layer in which a low-temperature buffer layer, a U-type gallium nitride GaN layer, an N-type GaN layer, a barrier layer / well layer / supplementary layer / slope well layer structure are sequentially formed from bottom to top on the substrate , functional layer, light emitting layer and P-type GaN layer.
[0037] Using the chemical vapor deposition method of metal organic compounds, at 550 ° C, the pressure of the reaction chamber is maintained at 300 mbar, and the flow rate of NH is 10000 sccm 3 , 50sccm TMGa, 100L / min H 2 1. Growing a low-temperature buffer layer GaN with a thickness of 20 nm on the substrate.
[0038] Grow a U-type GaN layer in the low-temperature buffer layer GaN: first grow a 2D-type GaN ...
Embodiment 2
[0048] h 2 Purify the substrate at high temperature in the environment; H at 1050°C 2 Under the atmosphere, feed 120L / min of H 2 , keep the reaction chamber pressure at 200mbar, and process the substrate for 9 minutes.
[0049] The epitaxial wafer includes a multi-quantum well layer in which a low-temperature buffer layer, a U-type gallium nitride GaN layer, an N-type GaN layer, a barrier layer / well layer / supplementary layer / slope well layer structure are sequentially formed from bottom to top on the substrate , functional layer, light emitting layer and P-type GaN layer.
[0050] Using the chemical vapor deposition method of metal organic compounds, at 570 ° C, the pressure of the reaction chamber is maintained at 450 mbar, and the flow rate of NH is 15000 sccm 3 , 75sccm TMGa, 120L / min H 2 1. Growing a low-temperature buffer layer GaN with a thickness of 20nm-40nm on the substrate.
[0051] Grow a U-type GaN layer in the low-temperature buffer layer GaN: first grow a 2D...
Embodiment 3
[0061] h 2 Purify the substrate at high temperature in the environment; H at 1100°C 2 Under the atmosphere, feed 130L / min of H 2 , keep the reaction chamber pressure at 300mbar, and process the substrate for 10min.
[0062] The epitaxial wafer includes a multi-quantum well layer in which a low-temperature buffer layer, a U-type gallium nitride GaN layer, an N-type GaN layer, a barrier layer / well layer / supplementary layer / slope well layer structure are sequentially formed from bottom to top on the substrate , functional layer, light emitting layer and P-type GaN layer.
[0063] Using the chemical vapor deposition method of metal organic compounds, at 580 ° C, the pressure of the reaction chamber is maintained at 600 mbar, and the flow rate of NH is 20000 sccm 3 , 100sccm TMGa, 130L / min H 2 1. Growing a low-temperature buffer layer GaN with a thickness of 40 nm on the substrate.
[0064] Grow a U-type GaN layer in the low-temperature buffer layer GaN: first grow a 2D-type G...
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