A kind of preparation method of porous oil-containing lubricating material
A technology of lubricating material and preparation steps, applied in the field of lubricating material preparation, can solve problems such as precipitation easily affected by the environment, uneven pore distribution, failure of lubricating material, etc., and achieve the effect of long-term effective lubrication, good bonding, and avoiding pollution
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example 1
[0020] First collect the fresh black fungus, wash it and dry it naturally, collect the dried black fungus and grind it, then mix the black fungus powder with the chitinase solution with an enzyme activity of 30U / mL at a mass ratio of 1:100 , heated in a water bath at 40°C for 1h; after the completion of the water bath heating, continue to heat up to 75°C, then incubate and inactivate the enzyme for 1h, then centrifuge at 6800r / min for 10min, collect the supernatant, and use a volume ratio of 1:4 , the supernatant was stirred and mixed with absolute ethanol, treated in an ice-water bath at 0°C for 6h, then centrifuged at 6000r / min for 10min, and the lower layer was collected and freeze-dried to prepare the black fungus polysaccharide; and calculated in parts by weight , respectively weighed 45 parts of deionized water, 10 parts of black fungus polysaccharide prepared above, and 5 parts of trisodium citrate were placed in a Erlenmeyer flask, heated in a water bath at 65°C for 25 ...
example 2
[0023]First collect the fresh black fungus, wash it and dry it naturally, collect the dried black fungus and grind it, then mix the black fungus powder with the chitinase solution with an enzyme activity of 30U / mL at a mass ratio of 1:100 , heated in a water bath at 43°C for 1.5h; after the completion of the water bath heating, continue to heat up to 75-80°C, then heat-preserve and inactivate the enzyme for 1.5h, then centrifuge at 6900r / min for 13min, collect the supernatant, and press the volume Mix the supernatant with absolute ethanol at a ratio of 1:4, treat it in an ice-water bath at 3°C for 7 hours, then centrifuge at 7000r / min for 13 minutes, collect the lower precipitate and freeze-dry to prepare the black fungus polysaccharide; then press In terms of parts by weight, weigh 48 parts of deionized water, 13 parts of black fungus polysaccharide prepared above, and 8 parts of trisodium citrate in a Erlenmeyer flask, heat in a water bath at 68°C for 280 minutes, and then ...
example 3
[0026] First collect the fresh black fungus, wash it and dry it naturally, collect the dried black fungus and grind it, then mix the black fungus powder with the chitinase solution with an enzyme activity of 30U / mL at a mass ratio of 1:100 , heated in a water bath at 45°C for 2h; after the completion of the water bath heating, continue to heat up to 80°C, then heat-preserve and inactivate the enzyme for 2h, then centrifuge at 7000r / min for 15min, collect the supernatant, and use a volume ratio of 1:4 , the supernatant was stirred and mixed with absolute ethanol, treated in an ice-water bath at 5°C for 8 hours, and then centrifuged at 8000r / min for 15 minutes, and the lower layer was collected and freeze-dried to prepare black fungus polysaccharides; and calculated in parts by weight , weighed 50 parts of deionized water, 15 parts of black fungus polysaccharide prepared above, and 10 parts of trisodium citrate were placed in a conical flask, heated in a water bath at 70°C for 30...
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Abstract
Description
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Application Information
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