Nitrogen-doped graphene loaded Pd/Ni catalyst and preparation method thereof
A nitrogen-doped graphene and catalyst technology, applied in physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve problems such as dispersibility, poor stability, easy agglomeration of composite catalysts, and catalytic activity to be improved. , to achieve high stability, high redox catalytic performance, and reduce the effect of agglomeration
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Embodiment 1
[0033] A nitrogen-doped graphene supported Pd / Ni catalyst, prepared from the following components by weight: NiSO 4 ·6H 2 1 part of O, 4 parts of nitrogen-doped graphene, 20 parts of potassium borohydride; also contains an appropriate amount of 0.05mol / L of PdCl 2 solution, so that the molar ratio of Ni to Pd is 1:2;
[0034] Wherein, nitrogen-doped graphene is made by following method:
[0035] Add graphene oxide into an appropriate amount of ammonia water and ultrasonically disperse for 10 minutes, then add the dispersed solution into a hydrothermal reaction kettle, and then react at a temperature of 200°C for 4 hours. Nitrogen-doped graphene was obtained by drying at ℃ for 10 hours; 150 ml of ammonia water was added to every 1 gram of graphene oxide.
[0036] A preparation method of nitrogen-doped graphene supported Pd / Ni catalyst, comprising the following steps:
[0037] a) adding nitrogen-doped graphene to distilled water for ultrasonic treatment to make it uniformly ...
Embodiment 2
[0044] A nitrogen-doped graphene supported Pd / Ni catalyst, prepared from the following components by weight: NiSO 4 ·6H 2 1 part of O, 5 parts of nitrogen-doped graphene, 23 parts of potassium borohydride; also contains an appropriate amount of 0.05mol / L of PdCl 2 solution, so that the molar ratio of Ni to Pd is 1:3;
[0045] Wherein, nitrogen-doped graphene is made by following method:
[0046]Add graphene oxide into an appropriate amount of ammonia water and ultrasonically disperse for 12 minutes, then add the dispersed solution into a hydrothermal reaction kettle, and then react at a temperature of 210°C for 5 hours. Nitrogen-doped graphene was obtained by drying at ℃ for 12 hours; wherein 150 ml of ammonia water was added to 1 gram of graphene oxide.
[0047] A preparation method of nitrogen-doped graphene supported Pd / Ni catalyst, comprising the following steps:
[0048] a) adding nitrogen-doped graphene to distilled water for ultrasonic treatment to make it uniformly...
Embodiment 3
[0055] A nitrogen-doped graphene supported Pd / Ni catalyst, prepared from the following components by weight: NiSO 4 ·6H 2 1 part of O, 6 parts of nitrogen-doped graphene, 25 parts of potassium borohydride; also contains an appropriate amount of 0.05mol / L of PdCl 2 solution, so that the molar ratio of Ni to Pd is 1:4;
[0056] Wherein, nitrogen-doped graphene is made by following method:
[0057] Add graphene oxide into an appropriate amount of ammonia water and ultrasonically disperse for 15 minutes, then add the dispersed solution into a hydrothermal reaction kettle, and then react at a temperature of 250°C for 6 hours. Nitrogen-doped graphene was obtained by drying at ℃ for 14 hours; wherein 150 ml of ammonia water was added to 1 gram of graphene oxide.
[0058] A preparation method of nitrogen-doped graphene supported Pd / Ni catalyst, comprising the following steps:
[0059] a) adding nitrogen-doped graphene to distilled water for ultrasonic treatment to make it uniforml...
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