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Organic silicon deep dyeing promoter and preparation method thereof

A technology of darkening agent and organic silicon, which is applied in the field of organic silicon darkening agent and its preparation, can solve the problems of poor dyeing and dark fabrics, and achieve darkening effect, good effect and good washability Effect

Active Publication Date: 2016-10-12
常州新光印染有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But a big disadvantage of polyester fiber is that it is poor in dyeing dark color, especially black and other dark fabrics. blurry visual effects

Method used

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  • Organic silicon deep dyeing promoter and preparation method thereof

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Comparison scheme
Effect test

Embodiment 1

[0020] A silicone darkening agent, prepared from the following ingredients in parts by weight: 1 part of nano silicon dioxide, 1 part of sodium silicate, 2 parts of cetyltrimethylammonium bromide, 1 part of dodecyl chloride 3 parts of ammonium, 0.1 part of potassium sorbate, 2 parts of methyl glucose sesquistearate, 3 parts of polyoxyethylene oleate, 0.1 part of tetramethylammonium hydroxide, 20 parts of octamethylcyclotetrasiloxane , 1 part of vinyltriethoxysilane, 1 part of vinyltrimethoxysilane, 0.2 part of phytic acid, 1 part of glacial acetic acid, and 100 parts of deionized water.

[0021] The preparation method of above-mentioned organosilicon deepening agent is:

[0022] Step 1: Mix cetyltrimethylammonium bromide, dodecylammonium chloride, methylglucose sesquistearate, polyoxyethylene oleate and deionized water, and stir for 30 minutes;

[0023] Step 2: Add nano-silica, sodium silicate and octamethylcyclotetrasiloxane, and stir at high speed for 10 minutes;

[0024] ...

Embodiment 2

[0030] A silicone darkening agent, prepared from the following ingredients in parts by weight: 1.5 parts of nano silicon dioxide, 2 parts of sodium silicate, 3 parts of cetyltrimethylammonium bromide, dodecyl chloride 4 parts of ammonium, 0.2 parts of potassium sorbate, 3 parts of methyl glucose sesquistearate, 4 parts of polyoxyethylene oleate, 0.15 parts of tetramethylammonium hydroxide, 25 parts of octamethylcyclotetrasiloxane , 1.5 parts of vinyltriethoxysilane, 1-2 parts of vinyltrimethoxysilane, 0.35 parts of phytic acid, 1.5 parts of glacial acetic acid, and 125 parts of deionized water.

[0031] The preparation method of above-mentioned organosilicon deepening agent is:

[0032] Step 1: Mix cetyltrimethylammonium bromide, dodecylammonium chloride, methylglucose sesquistearate, polyoxyethylene oleate and deionized water, and stir for 40 minutes;

[0033] Step 2: Add nano-silica, sodium silicate and octamethylcyclotetrasiloxane, and stir at high speed for 20 minutes;

...

Embodiment 3

[0040] A silicone darkening agent, prepared from the following ingredients in parts by weight: 2 parts of nano silicon dioxide, 3 parts of sodium silicate, 4 parts of cetyltrimethylammonium bromide, dodecyl chloride 5 parts ammonium, 0.3 parts potassium sorbate, 4 parts methyl glucose sesquistearate, 5 parts polyoxyethylene oleate, 0.2 parts tetramethylammonium hydroxide, 30 parts octamethylcyclotetrasiloxane , 2 parts of vinyltriethoxysilane, 2 parts of vinyltrimethoxysilane, 0.5 part of phytic acid, 2 parts of glacial acetic acid, 150 parts of deionized water.

[0041] The preparation method of above-mentioned organosilicon deepening agent is:

[0042] Step 1: Mix cetyltrimethylammonium bromide, dodecylammonium chloride, methylglucose sesquistearate, polyoxyethylene oleate and deionized water, and stir for 50 minutes;

[0043] Step 2: Add nano-silica, sodium silicate and octamethylcyclotetrasiloxane, and stir at high speed for 30 minutes;

[0044] Step 3: Add vinyltriethox...

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Abstract

The invention provides an organic silicon deep dyeing promoter and a preparation method thereof. The organic silicon deep dyeing promoter is prepared by the following steps: firstly mixing hexadecyl trimethyl ammonium bromide, dodecyl ammonium chloride, methyl glucose sesquistearate and oleic acid polyoxyethylene ester with deionized water, and mixing for 30-50 minutes; adding nanosilicon dioxide, sodium silicate and octamethylcyclotetrasiloxane, and stirring for 10-30 minutes at high speed; adding vinyl triethoxysilane and vinyl trimethoxy silane, continuously stirring for 10-20 mintues at high speed, homogenizing for 10-30 minutes, and heating to 80-85 DEG C; adding tetramethylammonium hydroxide, stirring for 5-10 minutes, preserving the temperature for 3-4 hours, and cooling down; adding potassium sorbate and phytic acid, and stirring for 10-20 minutes; and finally adding glacial acetic acid to neutralize to be neutral, thereby obtaining the organic silicon deep dyeing promoter. The prepared organic silicon deep dyeing promoter has relatively lower brightness value, excellent deep dyeing promotion effect, and also has excellent wash resistance.

Description

technical field [0001] The invention relates to the field of textile materials, in particular to a silicone darkening agent and a preparation method thereof. Background technique [0002] Polyester fiber fabric is a synthetic fiber obtained by spinning polyester, which is formed by polycondensation of organic dibasic acid and dibasic alcohol. Compared with other textile fabrics, it has many advantages, such as low price, high strength, and strong heat resistance. , high dimensional stability, strong wrinkle resistance and good color fastness and other excellent characteristics, it is currently the most widely used synthetic fiber in the textile industry. But a big disadvantage of polyester fiber is that it is poor in dyeing dark color, especially black and other dark fabrics. Boundless visual effects. Especially in recent years, the production of fine and superfine polyester fibers and the appearance of polyester fiber imitation silk products have been welcomed and sought ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/673D06P1/66D06P1/613D06P1/651D06P1/653
CPCD06P1/6136D06P1/651D06P1/6533D06P1/66D06P1/67383
Inventor 潘明华
Owner 常州新光印染有限公司
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