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A kind of preparation method of fluorescent powder emitting red light

A red-light phosphor, red-emitting technology, applied in the directions of luminescent materials, chemical instruments and methods, etc., can solve the problems of short device life, poor anti-ultraviolet light performance, and difficulty in forming the phosphor film of the LED light-emitting layer, and achieve high precision High, accurate and informative data, good purity

Active Publication Date: 2018-08-17
TAIYUAN UNIV OF TECH
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Problems solved by technology

[0005] At present, the synthesis of red light phosphors is mainly based on the rare earth metal Eu as the central ion and the polymer material as the matrix to prepare red light materials. Although its luminous performance has been improved, there are still LED light-emitting layer phosphors made of it. Defects of difficult film formation, poor UV resistance, and short device life

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  • A kind of preparation method of fluorescent powder emitting red light
  • A kind of preparation method of fluorescent powder emitting red light
  • A kind of preparation method of fluorescent powder emitting red light

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Embodiment Construction

[0058] The present invention will be further described below in conjunction with accompanying drawing

[0059] figure 1 As shown, the state diagram for the preparation of the polymer, the position of each part must be correct, the proportion should be proportioned, and the operations should be performed in sequence.

[0060] Quantities of chemicals used in preparation are determined in pre-set ranges in grams, milliliters, centimeters 3 is the unit of measurement.

[0061] The preparation of the polymer is carried out in a three-necked flask, which is completed in a water bath, heating, magnetic stirring, nitrogen protection, and water circulation condensation;

[0062] The electric heater 1 is vertical, and the upper part of the electric heater 1 is a water bath 2, and the upper part of the water bath 2 is a three-necked flask 3, which is fixed by a fixed frame 21. The water bath 2 is a water bath 4, and the water bath 4 needs Submerge 4 / 5 of the volume of the three-necked...

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Abstract

The invention relates to a preparation method of red light emitting fluorescent powder. By aiming at the conditions of difficult film forming of red light fluorescent powder and poor ultraviolet light resistant performance, 2-thenoyltrifluoroacetone-phenanthroline-methacrylic acid-europium and (4-vinyl phenyl) trimethoxy silane is used as raw materials to prepare the red light emitting fluorescent powder through solution preparation, polymerization reaction, washing, suction filtration, vacuum freeze drying, grinding and screening. The preparation method has the advantages that the process is advanced; the data is precise, full and accurate; the prepared powder body material has high precision and good purity; the purity reaches 9.2 percent; the powder body particle diameter is less than or equal to 800nm; the chromaticity coordinate X is 0.625; Y is 0.308; red light is emitted out; the materials can be matched with blue and green luminous materials to be prepared into white light emitting light emitting diodes; the preparation method belongs to an advanced red light emitting fluorescent powder preparation method.

Description

technical field [0001] The invention relates to a method for preparing a phosphor powder emitting red light, and belongs to the technical field of preparation and application of luminescent materials. Background technique [0002] Silicone is the mainstream material of LED packaging materials, with Si-O-Si bond as the main chain and side chains containing organic groups, which have excellent heat resistance, UV resistance and processing performance. [0003] White light-emitting diodes (LEDs) are known as the fourth-generation green light sources because of their small size, low energy consumption, and long life, and have been widely used in industrial and civilian products. [0004] White light is a kind of composite light, which can be compounded by ultraviolet light to excite phosphors of red, green and blue three primary colors to obtain white light. Its color temperature and color rendering performance depend on the content of red light components. The role of color co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F230/08C08F230/04C09K11/06
CPCC08F230/04C08F230/08C09K11/06C09K2211/182
Inventor 张爱琴张怡宁贾虎生赵希瑾杨亚敏刘旭光许并社
Owner TAIYUAN UNIV OF TECH
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