High-voltage functional electrolyte and preparation method and application therefor
An electrolyte and high-voltage technology, which is used in the manufacture of electrolyte batteries, organic electrolytes, non-aqueous electrolytes, etc., can solve the problem that the structure of spinel nickel lithium manganate is not stable enough, the electrochemical performance of batteries is degraded, and the morphology of positive electrode materials is changed. problems, to achieve room temperature and high temperature cycle performance improvement, inhibition of further contact, inhibition of surface activity
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Embodiment 1
[0032] (1) Mix the cyclic carbonate solvent ethylene carbonate (EC) and the linear carbonate solvent ethyl methyl carbonate (EMC) at a volume ratio of EC:EMC=3:7, and use molecular sieves, calcium hydride, and lithium hydride to purify Remove impurities and water to obtain a mixed solvent;
[0033] (2) At room temperature, the conductive lithium salt LiPF 6 Dissolve in the solvent obtained in step (1), the final concentration is 1.0mol / L, and stir evenly to obtain a common electrolyte;
[0034] (3) Add diethyl (thiophen-2-ylmethyl) phosphate (the reagent is purchased from Adamas, the purity is greater than 98%, and is used without further purification) in the common electrolyte prepared in step (2), two The dosage of ethyl (thiophen-2-ylmethyl) phosphate is 0.25% of the mass of the electrolyte to obtain a high-voltage functional electrolyte for lithium ion batteries.
Embodiment 2
[0036] (1) Mix the cyclic carbonate solvent ethylene carbonate (EC) and the linear carbonate solvent ethyl methyl carbonate (EMC) at a volume ratio of EC:EMC=3:7, and use molecular sieves, calcium hydride, and lithium hydride to purify Remove impurities and water to obtain a mixed solvent;
[0037] (2) At room temperature, the conductive lithium salt LiPF 6 Dissolve in the solvent obtained in step (1), the final concentration is 1.0mol / L, and stir evenly to obtain a common electrolyte;
[0038] (3) Add diethyl (thiophen-2-ylmethyl) phosphate (the reagent is purchased from Adamas, the purity is greater than 98%, and is used without further purification) in the common electrolyte prepared in step (2), two The consumption of ethyl (thiophen-2-ylmethyl) phosphate is 0.5% of the mass of the electrolyte to obtain a high-voltage functional electrolyte for lithium ion batteries.
Embodiment 3
[0040] (1) Mix the cyclic carbonate solvent ethylene carbonate (EC) and the linear carbonate solvent ethyl methyl carbonate (EMC) at a volume ratio of EC:EMC=3:7, and use molecular sieves, calcium hydride, and lithium hydride to purify Remove impurities and water to obtain a mixed solvent;
[0041] (2) At room temperature, the conductive lithium salt LiPF 6 Dissolve in the solvent obtained in step (1), the final concentration is 1.0mol / L, and stir evenly to obtain a common electrolyte;
[0042](3) Add diethyl (thiophen-2-ylmethyl) phosphate (the reagent is purchased from Adamas, the purity is greater than 98%, and is used without further purification) in the common electrolyte prepared in step (2), two The amount of ethyl (thiophen-2-ylmethyl) phosphate is 1% of the mass of the electrolyte to obtain a high-voltage functional electrolyte for lithium ion batteries.
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