Micro-expansive coral sand concrete and preparation method thereof
A coral sand and micro-expansion technology, applied in the field of building materials, can solve the problems of poor long-term durability of coral sand concrete, poor volume stability of concrete, rapid drying shrinkage due to water demand, etc., to improve drying shrinkage and volume stability, guaranteeing Volume stability, the effect of compensating for porosity
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Embodiment 1
[0031] Add 115 parts of stearic acid, 120 parts of sodium hydroxide, and 0.5 parts of absolute ethanol into the flask, heat and stir evenly, control the heating temperature to 70°C, and the reaction time is 7h;
[0032] Add saturated sodium chloride to precipitate sodium stearate, raise the temperature to 85°C, add 0.08 parts of aliphatic amine polyoxyethylene ether, 0.03 parts of alkylbenzene sulfonate, fully react for 1 hour, and then cool to room temperature;
[0033] Add 50 parts of hydrochloric acid to neutralize until the pH is 6.7, and filter to separate and remove impurities to obtain an emulsion, which is the liquid expansion agent.
Embodiment 2
[0035] Add 96 parts of oleic acid, 105 parts of sodium hydroxide, 0.2 parts of absolute ethanol, and 0.1 part of ethylene glycol into the flask, heat and stir evenly, control the heating temperature to 65°C, and the reaction time to 6.5h;
[0036] Add saturated sodium chloride to precipitate sodium stearate, raise the temperature to 90°C, add 0.05 parts of alkylphenol polyoxyethylene ether and 0.04 parts of fatty alcohol polyoxyethylene ether, 0.02 parts of alkylbenzene sulfonate and 0.03 parts The alkylnaphthalene sulfonate, fully reacted for 1.5h and then cooled to room temperature;
[0037] Add 45 parts of hydrochloric acid to neutralize until the pH is 6.9, and filter to separate and remove impurities to obtain an emulsion, which is the liquid expansion agent.
Embodiment 3
[0039] Add 85 parts of oleic acid and 35 parts of linoleic acid, 130 parts of sodium hydroxide, 0.5 parts of ethylene glycol and 0.3 parts of propylene glycol into the flask, heat and stir evenly, control the heating temperature to 70°C, and the reaction time is 7h ;
[0040] Add saturated sodium chloride to precipitate sodium stearate, raise the temperature to 85°C, add 0.03 parts of alkylphenol polyoxyethylene ether and 0.06 part of phenethylphenol polyoxyethylene ether, 0.05 part of alkyl sulfonate and 0.04 Parts of alkyl phosphate, fully reacted for 2h and then cooled to room temperature;
[0041] Add 70 parts of hydrochloric acid for neutralization until the pH is 6.8, and filter to separate and remove impurities to obtain an emulsion that is the liquid expansion agent.
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