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Method for producing high-specific-capacity shuttlelike copper oxide electrode material

A copper oxide and shuttle-shaped technology, applied in hybrid capacitor electrodes, copper oxide/copper hydroxide, nanotechnology, etc., can solve the problems of limited use, high cost, toxicity, etc., and achieve narrow particle size distribution, broad application prospects, highly responsive effect

Active Publication Date: 2016-06-29
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Ruthenium oxide has been extensively studied for active electrode applications due to its high theoretical capacity (approximately 2000FG -1 ) around 1.4V in the potential window, but their usefulness is limited due to the high integer cost and toxic nature

Method used

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  • Method for producing high-specific-capacity shuttlelike copper oxide electrode material
  • Method for producing high-specific-capacity shuttlelike copper oxide electrode material
  • Method for producing high-specific-capacity shuttlelike copper oxide electrode material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmolNa 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 300W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. Such as figure 1 Shown product is identified as copper oxide through X-ray powder diffraction; Carry out morphology analysis to copper oxide with scanning electron microscope (SEM), from figure 2 It can be seen that its morphology is nanoshuttle. Excellent electrochemical cycle performance and specific capacitance can be obtained from image 3 see.

Embodiment 2

[0037] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmolNa 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 200W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. The morphology of copper oxide was analyzed by transmission electron microscopy (TEM). Figure 4 It can be seen that its morphology is nanoshuttle.

Embodiment 3

[0039] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmolNa 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 400W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. The morphology of copper oxide was analyzed by transmission electron microscopy (TEM). Figure 5 It can be seen that its morphology is nanoshuttle.

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Abstract

The invention discloses a method for producing a high-specific-capacity shuttlelike copper oxide electrode material. The method comprises the steps of adding soluble carbonate and triethylamine to a copper saline solution, and conducting ultrasonic dispersion and microwave treatment, so that copper oxide nanoparticles having the special shuttlelike appearance are obtained. The method is high in efficiency, simple and easy to operate and meets the industrial production requirements; the obtained shuttlelike copper oxide nanoparticles have the advantages of being high in purity, uniform in particle size, excellent in electrochemical performance and have wide application prospect in the field of supercapacitor electrode materials.

Description

technical field [0001] The invention relates to a method for preparing a high specific capacity shuttle-shaped copper oxide electrode material, which belongs to the field of metal oxide nanometer material preparation. Background technique [0002] With the rapid development of the global economy, the depletion of fossil fuels and increasing environmental pollution, there is an urgent need for efficient, clean and sustainable energy sources, as well as new technologies related to energy conversion and storage. Therefore, supercapacitors (also known as electrochemical capacitors) are characterized by high power, faster response time and a near-infinite life cycle with reasonable energy density, which is the advantage of both traditional dielectric capacitance and energy storage batteries. electrical energy storage device. The current development direction of supercapacitors should focus on the use of environmentally friendly materials, increased power and energy density, and ...

Claims

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Application Information

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IPC IPC(8): C01G3/02B82Y40/00H01G11/46
CPCY02E60/13C01G3/02C01P2002/72C01P2004/03C01P2004/04C01P2004/40C01P2006/40H01G11/46
Inventor 刘小鹤刘涛马仁志邱冠周
Owner CENT SOUTH UNIV
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