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A kind of temperature control health care microcapsule and preparation method thereof

A technology of microcapsules and health care, applied in the direction of microcapsule preparation, microsphere preparation, rayon manufacturing, etc., can solve the problems of production efficiency decline, raw material cost increase, poor dispersibility, etc., to improve absorption, ensure taking comfort, The effect of increasing the release rate and far-infrared normal emissivity

Active Publication Date: 2019-01-08
钱殷超 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0013] The purpose of the present invention is to provide a temperature-controlled health-care microcapsule and its preparation method to achieve temperature-controlled health care, exert the long-lasting effect of functional powder, and solve the problem of production efficiency caused by poor dispersion of health-care functional fibers in the production process. Technical issues such as reduction in cost of raw materials, increase in raw material costs, degradation of the powder when it encounters acid, and at the same time improving the comfort of the product in winter

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] A method for preparing temperature-controlled health-care microcapsules, the steps of which are: preparing prepolymer—preparing health-care functional pearl powder and temperature-induced phase change material paraffin blended composite core material emulsion—polymerization reaction to form a film—washing and drying dry;

[0054] Wherein, the preparation prepolymer step is:

[0055] The melamine that is 1: 2: 2 by mass ratio, the formaldehyde solution that concentration is 37wt% (37% is the general specification of commercially available product) and distilled water are mixed, adjust pH value to 9 with triethanolamine and be warming up to 70 ℃, with 200r / / Slow stirring for 1 min until transparent viscous liquid; the total amount of prepolymer is based on 140% of the paraffin mass;

[0056] The steps for preparing the composite core material emulsion of health-care functional pearl powder and temperature-induced phase change material paraffin blend are as follows:

[...

Embodiment 2

[0063] A method for preparing temperature-controlled health-care microcapsules, the steps of which are: preparing a prepolymer——preparing health-care functional traditional Chinese medicine notoginseng powder and a temperature-induced phase change material paraffin blend composite core material emulsion—polymerization reaction to form a film— wash and dry;

[0064] Wherein, the preparation prepolymer step is:

[0065] Mix melamine with a mass ratio of 1:1.8:2, formaldehyde solution with a concentration of 37wt%, and distilled water, adjust the pH value to 9 with triethanolamine, heat up to 68°C, and stir at a slow speed of 300r / min until transparent and viscous Liquid; the total amount of prepolymer is calculated according to 160% of the paraffin mass;

[0066] The steps for preparing the composite core material emulsion of health-care functional traditional Chinese medicine Panax notoginseng powder and temperature-induced phase change material paraffin blending are as follow...

Embodiment 3

[0073] A method for preparing temperature-controlled health-care microcapsules, the steps of which are: preparing a prepolymer—preparing a health-care functional antibacterial powder and a temperature-induced phase change material n-octadecane blended composite core material emulsion—polymerization reaction to form a film— - washed and dried;

[0074] Wherein, the preparation prepolymer step is:

[0075] Mix melamine with a mass ratio of 1:1.6:1.8, formaldehyde solution with a concentration of 37wt%, and distilled water, adjust the pH value to 8.5 with triethanolamine, heat up to 70°C, and stir at a slow speed of 250r / min until transparent and viscous Liquid; the total amount of prepolymer is calculated by 150% of the mass of n-octadecane;

[0076] The steps for preparing the composite core emulsion of health-care functional antibacterial powder and temperature-induced phase change material n-octadecane are as follows:

[0077] At a temperature of 45°C, mix 280g n-octadecane...

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Abstract

The invention relates to a temperature-controllable health-care microcapsule and a preparation method thereof. The preparation method includes the preparation steps of prepolymer preparing, compound core emulsion preparing, film formation by polymerization reaction, washing and drying. The temperature-controllable health-care microcapsule consists of a compound core and a wall material composed of high-molecular polymers, wherein the compound core is formed by blending adsorption of health-care functional powder and temperature-dependent phase change materials, the weight ratio of the composite core to the wall material is 0.3-3 to 1, average grain size of the health-care functional powder is not less than 1.2 micrometers, and average grain size of the microcapsule is not less than 3 micrometers. The temperature-controllable health-care microcapsule has the advantages that owing to the temperature control function of the microcapsule, release rate of trace elements of the functional powder in winter can be increased, human body subcutaneous microcirculation is reinforced, and human bodies' absorption of health-care active ingredients is improved; comfortable temperature between a clothing product and the skin of human bodies can be kept; the problem of dispersibility of the functional powder in blended spinning production can be solved.

Description

technical field [0001] The invention belongs to the technical field of microcapsule preparation, and relates to a temperature-controlled health-care microcapsule suitable for the textile field and a preparation method thereof. Background technique [0002] Microcapsule technology is a new type of technology that uses film-forming materials to coat tiny active particles into particles with a core-wall-shell structure. Microencapsulation of tiny active materials can effectively reduce the reaction of active materials to surrounding systems, including solid, liquid, gas and light, and effectively control their flow, release or expansion to the external environment. At present, microcapsule technology has been widely used in food, medicine, textile and engineering materials and other fields. [0003] Chinese patent application number 200610017695 discloses a textile nano-finishing agent with persistent antibacterial and aromatic effects and its manufacturing process. It uses a ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J13/14C08G12/32D01F1/10
Inventor 钱殷超顾肇文
Owner 钱殷超
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