Method for preparing high-sensitivity nano-zirconia-doped dezocine molecular imprinting electrochemical sensor
A nano-zirconia and molecular imprinting technology, applied in the direction of material electrochemical variables, can solve the problems of inappropriate matching of functional monomers and template molecules, low sensitivity, and poor cross-linking rigidity.
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[0014] 1. Treatment of glassy carbon electrodes
[0015] Polish the glassy carbon electrode on a polishing cloth with 1.0 μm, 0.3 μm and 0.05 μm alumina powder in turn, then put it into nitric acid with a volume ratio of 1:1 for 8 minutes, then put it into absolute ethanol for 8 minutes, and finally Ultrasonic cleaning with pure water.
[0016] 2. Preparation of dezocine molecularly imprinted electrochemical sensor
[0017] To 10.0mL solvent ethanol, add 0.4mmol template molecule dezocine, 2.0mmol functional monomer (5s, 8s)-3-(4'-chloro-3'-fluoro-4-propenylbiphenyl) -3-yl)-4-hydroxyl-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, 5mmol crosslinking agent maleic rosin ethylene glycol acrylate, 0.25mmol initiation Azobisisobutyronitrile and 0.0350g of nano-zirconia, each chemical reagent added ultrasonically dissolved for 9 minutes;
[0018] Take 8 μL of the mixture in step and apply it on the surface of a clean and smooth glassy carbon electrode with a diameter of 2 mm. The t...
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