Adhesive layer with separator, method for producing same, polarizing film with adhesive layer with separator, method for producing polarizing film with adhesive layer with separator, and image display device
A technology of adhesive layer and manufacturing method, which is applied in the field of polarizing film, and achieves the effect of excellent processability
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[0152] Hereinafter, the present invention will be described more specifically by way of examples, but the present invention is not limited to these examples. Parts and % in each example are based on weight.
[0153]
[0154] The weight-average molecular weight of the hydroxyl group-containing (meth)acrylic polymer (A) is measured by GPC (gel permeation chromatography). Analytical device: HLC-8120GPC manufactured by Tosoh Corporation; column: G7000HXL+GMHXL+GMHXL manufactured by Tosoh Corporation; column dimensions: 7.8mmφ×30cm each, 90cm in total; column temperature: 40°C; flow rate: 0.8ml / min; injection volume: 100μl; eluent: tetrahydrofuran; detector: differential refractometer (RI); standard sample: polystyrene
[0155]
[0156] In order to produce a thin polarizer, first, a laminate formed by forming a PVA layer with a thickness of 9 μm on an amorphous PET substrate is assisted in stretching in an air atmosphere at a stretching temperature of 130°C to form a stretche...
manufacture example 1
[0164]
[0165] Add 99 parts of butyl acrylate, 1 part of 4-hydroxybutyl acrylate (HBA), and 100 parts of monomer (solid content) to a reaction vessel with a cooling pipe, nitrogen gas introduction pipe, thermometer and stirring device together with ethyl acetate. Parts are 1 part of AIBN as an initiator, reacted at 60° C. for 7 hours under a nitrogen stream, and then added ethyl acetate to the reaction solution to obtain a hydroxyl-containing (meth)acrylic acid with a weight average molecular weight of 1.6 million. A solution of a polymeroid (A-1) (solid content concentration: 30% by weight). Table 2 shows the compounding and molecular weight of the (meth)acrylic polymer (A-1).
manufacture example 2
[0167]
[0168] ( A solution of a meth)acrylic polymer (A-2). Table 2 shows the compounding and molecular weight of the (meth)acrylic polymer (A-2).
PUM
Property | Measurement | Unit |
---|---|---|
Adhesion | aaaaa | aaaaa |
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