Fat globule membrane powder, preparation method and application thereof
A fat globule membrane and membrane material technology, applied in the field of fat globule membrane powder and its preparation, can solve the problems of destroying the natural structure of the fat globule membrane powder, affecting the emulsifying performance and nutritional properties, and the separation method being time-consuming and labor-intensive, and achieving a good application prospect. , good storage stability, the effect of reducing production costs
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Embodiment 1
[0026] 1. The preparation method of fat globule film powder is:
[0027] (1) Get 20kg of fresh buttermilk, add sodium citrate, and adjust the pH to be 7;
[0028] (2) The material obtained in step (1) is separated and concentrated using a 0.1 μm cellulose ester film, and concentrated to 1 / 4 times the original volume, that is, the retentate is 5 kg and then stopped. 15kg of deionized water was added to the intercepted end, and this step was repeated 3 times. The temperature of membrane separation, concentration and diafiltration is both 50°C and the pressure is 0.5MPa;
[0029] (3) Freeze-dry the retentate after membrane separation and concentration to obtain fat globule membrane powder. Among them, the total protein content is 50%, the lipid content is 40%, the moisture content is 5%, and the ash content is 5%. Among them, the fat globule membrane protein, casein and whey protein account for 68% and 70% of the total protein respectively. % and 25%.
[0030] 2. Preparation ...
Embodiment 2
[0037] 1. The preparation method of fat globule membrane powder:
[0038] (1) Reconstitute 24kg of buttermilk powder into an 8% solution, stir at 35°C for 90 minutes, cool to 4-7°C and refrigerate overnight, then add sodium tartrate to adjust the pH to 8;
[0039] (2) The material obtained in step (1) is separated and concentrated using a 1.5 μm regenerated cellulose membrane, and concentrated to 1 / 6 times the original volume, that is, the retentate is 4 kg and then stopped. 20kg of deionized water was added to the intercepted end, and this step was repeated 5 times. The temperature of membrane separation, concentration and diafiltration is both 10°C and the pressure is 0.7MPa;
[0040] (3) Freeze-dry the retentate after membrane separation and concentration to obtain fat globule membrane powder. Wherein, the total protein content is 60%, the lipid content is 34%, the moisture content is 3%, and the ash content is 3%. Among them, fat globule membrane protein, casein and whe...
Embodiment 3
[0048]1. The preparation method of fat globule membrane powder is:
[0049] (1) Reconstitute 25 kg of buttermilk powder into a 9% solution, stir at 45°C for 30 minutes, cool to 4-7°C and refrigerate overnight, then add sodium acetate to adjust the pH to 8;
[0050] (2) The material obtained in step (1) is separated and concentrated using a 0.4 μm ceramic membrane, and concentrated to 1 / 5 times the original volume, that is, the retentate is 5 kg and then stopped. 20kg of deionized water was added to the intercepted end, and this step was repeated 4 times. The temperature of membrane separation, concentration and diafiltration is both 30°C and the pressure is 0.6MPa;
[0051] (3) Freeze-dry the retentate after membrane separation and concentration to obtain fat globule membrane powder. Wherein, the total protein content is 55%, the lipid content is 35%, the water content is 5% and the ash content is 5%. Among them, fat globule membrane protein, casein and whey protein account...
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