Reactor for synthesis of alkylate oil

An alkylate oil and reactor technology, applied in the directions of hydrocarbons, hydrocarbons, chemical instruments and methods, etc., can solve problems such as acid-hydrocarbon contact problems, reduce alkene ratio, speed up reaction rate, and strictly control The effect of reaction temperature

Active Publication Date: 2015-11-18
TIANJIN UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The purpose of the present invention is to provide a reactor for the synthesis of alkylated oil that can solve the

Method used

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  • Reactor for synthesis of alkylate oil

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Effect test

Embodiment 1

[0015] Use the reactor for the synthesis of alkylate oil of the present invention to carry out the synthesis reaction of alkylate oil. A small-scale experimental device is used. The diameter of the straight cylinder section is 80mm and the height is 1600mm.

[0016] The diameter of the wide diameter section is 200mm and the height is 500mm.

[0017] The height of the transition section is 150mm.

[0018] 1 downcomer, downcomer diameter 14mm, length 1500mm,

[0019] 3 outer tubes, the diameter of the outer tube is 9mm, the tube length is 1500mm, it is a smooth tube;

[0020] 3 inner tubes, the inner tube diameter is 5mm, the tube length is 700mm,

[0021] The distance between the lower tube sheet of the inner tube and the lower tube sheet of the outer tube is 100 mm, and no filler is set in the space inside the outer tube and outside the inner tube.

[0022] Small holes are uniformly arranged on the inner tube throughout the axial length, with a diameter of 0.5mm.

[0023] ...

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Abstract

The invention discloses a reactor for synthesis of alkylate oil. The reactor is composed of a straight tube section, a wide radius section and a transition section between the straight tube section and the wide radius section. An inner pipe lower pipe plate is disposed at the lower part of the straight tube section, an outer pipe lower pipe plate is arranged above the inner pipe lower pipe plate, and an upper pipe plate is arranged at the joint of the straight tube section and the transition section. The upper end and lower end of a downcomer are respectively connected to the upper pipe plate and the outer pipe lower pipe plate, the outer pipe upper end and lower end are respectively connected to the upper pipe plate and the outer pipe lower pipe plate, the inner pipe is disposed inside the outer pipe, the upper end of the inner pipe is a blind end, the lower end of the inner pipe is connected to the inner pipe lower pipe plate, and the inner pipe is provided with holes. Compared with existing industrial reactors, the reactor provided by the invention has better acid hydrocarbon contact effect, accelerates the reaction rate, reduces the reactor size, at the same time lowers alkyl-olefin ratio, and can strictly control the reaction temperature and reduce reaction by-product, thereby increasing the yield and quality of alkylate synthetic oil, and reducing the energy consumption needed by isobutane circulation.

Description

technical field [0001] The invention relates to chemical equipment, in particular to a reactor for synthesis of alkylated oil. Background technique [0002] The industrial isooctane produced by the alkylation reaction of C4 olefins and isobutane is a blending component of high-octane gasoline with various trimethylpentane as the main component. Industrial isooctane has a high octane number and combustion The advantages of less harmful products and lower vapor pressure. Alkylation reaction can be divided into sulfuric acid alkylation process and hydrofluoric acid alkylation process according to the catalyst used. Hydrofluoric acid is a volatile and highly toxic chemical. Once leaked, it will cause serious harm to the environment and production. The main disadvantage of the sulfuric acid alkylation process is the large discharge of waste acid. The sulfuric acid alkylation process is mostly used in my country. It is generally believed that the control step that determines the...

Claims

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Application Information

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IPC IPC(8): C10G50/00C07C2/62C07C9/16
Inventor 张敏卿张金利徐钦李文鹏
Owner TIANJIN UNIV
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